2,5-dideoxy-1-O-methyl-3-O-(tert-butyldiphenylsilyl)-5-iodo-D-ribonolactone

Base Information

Chemical Name:2,5-dideoxy-1-O-methyl-3-O-(tert-butyldiphenylsilyl)-5-iodo-D-ribonolactone
CAS No.:951766-59-9
Molecular Formula:C₂₁H₂₅IO₃Si
Molecular Weight:480.418
Hs Code.:

Synonyms:2,5-dideoxy-1-O-methyl-3-O-(tert-butyldiphenylsilyl)-5-iodo-D-ribonolactone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,5-dideoxy-1-O-methyl-3-O-(tert-butyldiphenylsilyl)-5-iodo-D-ribonolactone

Chemical Property:

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Technology Process of 2,5-dideoxy-1-O-methyl-3-O-(tert-butyldiphenylsilyl)-5-iodo-D-ribonolactone

There total 4 articles about 2,5-dideoxy-1-O-methyl-3-O-(tert-butyldiphenylsilyl)-5-iodo-D-ribonolactone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 951766-57-7
2-deoxy-1-O-methyl-3-O-(tert-butyldiphenylsilyl)-5-O-(p-toluenesulfonyl)-D-ribonolactone

: 951766-59-9
2,5-dideoxy-1-O-methyl-3-O-(tert-butyldiphenylsilyl)-5-iodo-D-ribonolactone

Guidance literature:: With sodium iodide; In acetone; Heating;
DOI:10.1021/jo0712143

Reference yield:

: 951766-55-5
2-deoxy-1-O-methyl-3-O-(tert-butyldiphenylsilyl)-5-O-(p-toluenesulfonyl)-D-ribofuranose

: 951766-59-9
2,5-dideoxy-1-O-methyl-3-O-(tert-butyldiphenylsilyl)-5-iodo-D-ribonolactone

Guidance literature:: Multi-step reaction with 2 steps

1: 71 percent / 3-chloroperbenzoic acid; indium(III) trifluoromethanesulfonate / CH₂Cl₂ / 20 °C

2: 100 percent / sodium iodide / acetone / Heating

With indium(III) triflate; 3-chloro-benzenecarboperoxoic acid; sodium iodide; In dichloromethane; acetone;
DOI:10.1021/jo0712143

Reference yield:

: 10437-39-5
methyl 2-deoxy-5-O-(p-toluenesulfonyl)-α,β-D-erythro-pentofuranoside

: 951766-59-9
2,5-dideoxy-1-O-methyl-3-O-(tert-butyldiphenylsilyl)-5-iodo-D-ribonolactone

Guidance literature:: Multi-step reaction with 3 steps

1: 85 percent / imidazole / dimethylformamide / 20 °C

2: 71 percent / 3-chloroperbenzoic acid; indium(III) trifluoromethanesulfonate / CH₂Cl₂ / 20 °C

3: 100 percent / sodium iodide / acetone / Heating

With indium(III) triflate; 1H-imidazole; 3-chloro-benzenecarboperoxoic acid; sodium iodide; In dichloromethane; N,N-dimethyl-formamide; acetone;
DOI:10.1021/jo0712143