1-O,2-S-(2-acetyl-1-methyl-1,2-ethenediyl)-3,4,6-tri-O-benzyl-2-thio-α-D-glucopyranose

Base Information

Chemical Name:1-O,2-S-(2-acetyl-1-methyl-1,2-ethenediyl)-3,4,6-tri-O-benzyl-2-thio-α-D-glucopyranose
CAS No.:152420-91-2
Molecular Formula:C₃₂H₃₄O₆S
Molecular Weight:546.684
Hs Code.:

Synonyms:1-O,2-S-(2-acetyl-1-methyl-1,2-ethenediyl)-3,4,6-tri-O-benzyl-2-thio-α-D-glucopyranose

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Chemical Property of 1-O,2-S-(2-acetyl-1-methyl-1,2-ethenediyl)-3,4,6-tri-O-benzyl-2-thio-α-D-glucopyranose

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Technology Process of 1-O,2-S-(2-acetyl-1-methyl-1,2-ethenediyl)-3,4,6-tri-O-benzyl-2-thio-α-D-glucopyranose

There total 9 articles about 1-O,2-S-(2-acetyl-1-methyl-1,2-ethenediyl)-3,4,6-tri-O-benzyl-2-thio-α-D-glucopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 55628-54-1
3,4,6-tri-O-benzyl-D-glucal

: 107552-89-6
3-thiophthalimide-2,4-pentanedione

: 152420-91-2
1-O,2-S-(2-acetyl-1-methyl-1,2-ethenediyl)-3,4,6-tri-O-benzyl-2-thio-α-D-glucopyranose

Guidance literature:: With 2,6-dimethylpyridine; 3 Angstroem MS; Ambient temperature;
DOI:10.1021/jo981047u

Reference yield: 83.0%

: 55628-54-1
3,4,6-tri-O-benzyl-D-glucal

: 152420-82-1
2-((E)-1-Acetyl-2-hydroxy-propenylsulfanyl)-isoindole-1,3-dione

: 152420-91-2
1-O,2-S-(2-acetyl-1-methyl-1,2-ethenediyl)-3,4,6-tri-O-benzyl-2-thio-α-D-glucopyranose

Guidance literature:: With 2,6-dimethylpyridine; In chloroform; for 96h; Ambient temperature;
DOI:10.1021/jo00125a030

Reference yield: 42.0%

: 55628-54-1
3,4,6-tri-O-benzyl-D-glucal

: 107552-89-6
3-thiophthalimide-2,4-pentanedione

: 152420-91-2
1-O,2-S-(2-acetyl-1-methyl-1,2-ethenediyl)-3,4,6-tri-O-benzyl-2-thio-α-D-glucopyranose

: 214001-50-0
1-O,2-S-(2-acetyl-1-methyl-1,2-ethenediyl)-3,4,6-tri-O-benzyl-2-thio-β-D-mannopyranose

Guidance literature:: With 2,6-dimethylpyridine; 3 Angstroem MS; In dimethyl sulfoxide; for 168h; Product distribution; Ambient temperature; other solvents;
DOI:10.1021/jo981047u