Technology Process of C45H57N3O9S
There total 6 articles about C45H57N3O9S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1: pyridine / 14 h / Ambient temperature
2: 15 g / t-BuOK / dimethylformamide / 12 h / Ambient temperature
3: p-TsOH / benzene / 3 h / Heating
4: 19 g / m-chloroperbenzoic acid (m-CPBA) / CH2Cl2 / 1.) < 30 deg C, 2.) room temperature, 1,5 h
5: 1.) ethylmagnesium bromide / 1.) benzene, 15 min, room temperature, 2.) 2,5 h, room temperature
With
pyridine; ethylmagnesium bromide; potassium tert-butylate; toluene-4-sulfonic acid; 3-chloro-benzenecarboperoxoic acid;
In
dichloromethane; N,N-dimethyl-formamide; benzene;
DOI:10.1021/jo00186a014
- Guidance literature:
-
Multi-step reaction with 3 steps
1: p-TsOH / benzene / 3 h / Heating
2: 19 g / m-chloroperbenzoic acid (m-CPBA) / CH2Cl2 / 1.) < 30 deg C, 2.) room temperature, 1,5 h
3: 1.) ethylmagnesium bromide / 1.) benzene, 15 min, room temperature, 2.) 2,5 h, room temperature
With
ethylmagnesium bromide; toluene-4-sulfonic acid; 3-chloro-benzenecarboperoxoic acid;
In
dichloromethane; benzene;
DOI:10.1021/jo00186a014
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 19 g / m-chloroperbenzoic acid (m-CPBA) / CH2Cl2 / 1.) < 30 deg C, 2.) room temperature, 1,5 h
2: 1.) ethylmagnesium bromide / 1.) benzene, 15 min, room temperature, 2.) 2,5 h, room temperature
With
ethylmagnesium bromide; 3-chloro-benzenecarboperoxoic acid;
In
dichloromethane;
DOI:10.1021/jo00186a014
