3-(1-(2,4-dichlorobenzyl)-3-(methoxymethoxy)-1H-pyrazole-5-yl)propane-1-ol

Base Information

• Chemical Name: 3-(1-(2,4-dichlorobenzyl)-3-(methoxymethoxy)-1H-pyrazole-5-yl)propane-1-ol
• CAS No.: 888738-88-3
• Molecular Formula: C₁₅H₁₈Cl₂N₂O₃
• Molecular Weight: 345.226

Synonyms:3-(1-(2,4-dichlorobenzyl)-3-(methoxymethoxy)-1H-pyrazole-5-yl)propane-1-ol

Chemical Property of 3-(1-(2,4-dichlorobenzyl)-3-(methoxymethoxy)-1H-pyrazole-5-yl)propane-1-ol

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Technology Process of 3-(1-(2,4-dichlorobenzyl)-3-(methoxymethoxy)-1H-pyrazole-5-yl)propane-1-ol

There total 2 articles about 3-(1-(2,4-dichlorobenzyl)-3-(methoxymethoxy)-1H-pyrazole-5-yl)propane-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

ethyl 3-[1-(2,4-dichlorobenzyl)-3-(methoxymethoxy)-1H-pyrazol-5-yl]propanoate (888738-87-2) + ammonium chloride → 3-(1-(2,4-dichlorobenzyl)-3-(methoxymethoxy)-1H-pyrazole-5-yl)propane-1-ol (888738-88-3)

Guidance literature:

With diisobutylaluminium hydride; In tetrahydrofuran; ethanol; toluene;

Reference yield: 97.0%

ethyl 3-[1-(2,4-dichlorobenzyl)-3-(methoxymethoxy)-1H-pyrazol-5-yl]propanoate (888738-87-2) → 3-(1-(2,4-dichlorobenzyl)-3-(methoxymethoxy)-1H-pyrazole-5-yl)propane-1-ol (888738-88-3)

Guidance literature:

With diisobutylaluminium hydride; In tetrahydrofuran; toluene; at 0 - 20 ℃; for 1h;

Reference yield: 95.0%

(2-hydroxy-3-methoxyphenyl)acetic acid methyl ester (103324-26-1) + 3-(1-(2,4-dichlorobenzyl)-3-(methoxymethoxy)-1H-pyrazole-5-yl)propane-1-ol (888738-88-3) + 1,1'-(Azodicarbonyl)dipiperidin (10465-81-3,871024-86-1) → (2-{3-[1-(2,4-dichlorobenzyl)-3-(methoxymethoxy)-1H-pyrazole-5-yl]propoxy}-3-methoxyphenyl)acetic acid methyl ester

Guidance literature:

With tributylphosphine; In tetrahydrofuran; di-isopropyl ether;

upstream raw materials:

ethyl 3-[1-(2,4-dichlorobenzyl)-3-(methoxymethoxy)-1H-pyrazol-5-yl]propanoate

Downstream raw materials:

(1-benzyl-3-{3-[1-(2,4-dichlorobenzyl)-3-(methoxymethoxy)-1H-pyrazol-5-yl]propoxy}-1H-pyrazol-4-yl)acetic acid

(2-{3-[1-(2,4-dichlorobenzyl)-3-(methoxymethoxy)-1H-pyrazol-5-yl]propoxy}pyridin-3-yl)acetic acid

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