1-Methyl-4-(4-{4-methyl-3-[(Z)-phenylimino]-6-[(E)-phenylimino]-cyclohexa-1,4-dienyl}-phenyl)-6-[(Z)-phenylimino]-3-[(E)-phenylimino]-cyclohexa-1,4-diene

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Chemical Name:1-Methyl-4-(4-{4-methyl-3-[(Z)-phenylimino]-6-[(E)-phenylimino]-cyclohexa-1,4-dienyl}-phenyl)-6-[(Z)-phenylimino]-3-[(E)-phenylimino]-cyclohexa-1,4-diene
CAS No.:495383-61-4
Molecular Formula:C₄₄H₃₄N₄
Molecular Weight:618.781
Hs Code.:

Synonyms:1-Methyl-4-(4-{4-methyl-3-[(Z)-phenylimino]-6-[(E)-phenylimino]-cyclohexa-1,4-dienyl}-phenyl)-6-[(Z)-phenylimino]-3-[(E)-phenylimino]-cyclohexa-1,4-diene

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Chemical Property of 1-Methyl-4-(4-{4-methyl-3-[(Z)-phenylimino]-6-[(E)-phenylimino]-cyclohexa-1,4-dienyl}-phenyl)-6-[(Z)-phenylimino]-3-[(E)-phenylimino]-cyclohexa-1,4-diene

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Technology Process of 1-Methyl-4-(4-{4-methyl-3-[(Z)-phenylimino]-6-[(E)-phenylimino]-cyclohexa-1,4-dienyl}-phenyl)-6-[(Z)-phenylimino]-3-[(E)-phenylimino]-cyclohexa-1,4-diene

There total 5 articles about 1-Methyl-4-(4-{4-methyl-3-[(Z)-phenylimino]-6-[(E)-phenylimino]-cyclohexa-1,4-dienyl}-phenyl)-6-[(Z)-phenylimino]-3-[(E)-phenylimino]-cyclohexa-1,4-diene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 495383-60-3
4,4''-dimethyl-N²,N⁵,N^2''_,N5''-tetraphenyl-[1,1';4',1'']terphenyl-2,5,2'',5''-tetraamine

: 495383-61-4
1-Methyl-4-(4-{4-methyl-3-[(Z)-phenylimino]-6-[(E)-phenylimino]-cyclohexa-1,4-dienyl}-phenyl)-6-[(Z)-phenylimino]-3-[(E)-phenylimino]-cyclohexa-1,4-diene

Guidance literature:: With calcium hypochlorite; In dichloromethane; at 20 ℃; for 4h;
DOI:10.1246/bcsj.75.1827

Reference yield:

: 4612-26-4
1,4-Phenyldiboronic acid

: 495383-61-4
1-Methyl-4-(4-{4-methyl-3-[(Z)-phenylimino]-6-[(E)-phenylimino]-cyclohexa-1,4-dienyl}-phenyl)-6-[(Z)-phenylimino]-3-[(E)-phenylimino]-cyclohexa-1,4-diene

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / Pd(P(C₆H₅)3)4; Na₂CO₃ / dimethylformamide; H₂O / 16 h / 70 °C

2: 98 percent / Ca(OCl)2 / CH₂Cl₂ / 4 h / 20 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; calcium hypochlorite; sodium carbonate; In dichloromethane; water; N,N-dimethyl-formamide; 1: Suzuki coupling;
DOI:10.1246/bcsj.75.1827

Reference yield:

: 13070-25-2
2-bromo-5-methyl-[1,4]benzoquinone

: 495383-61-4
1-Methyl-4-(4-{4-methyl-3-[(Z)-phenylimino]-6-[(E)-phenylimino]-cyclohexa-1,4-dienyl}-phenyl)-6-[(Z)-phenylimino]-3-[(E)-phenylimino]-cyclohexa-1,4-diene

Guidance literature:: Multi-step reaction with 3 steps

1: 56 percent / TiCl₄ / chlorobenzene / 24 h / 135 °C

2: 80 percent / Pd(P(C₆H₅)3)4; Na₂CO₃ / dimethylformamide; H₂O / 16 h / 70 °C

3: 98 percent / Ca(OCl)2 / CH₂Cl₂ / 4 h / 20 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; calcium hypochlorite; titanium tetrachloride; sodium carbonate; In dichloromethane; water; N,N-dimethyl-formamide; chlorobenzene; 2: Suzuki coupling;
DOI:10.1246/bcsj.75.1827