3-[(1S,4aR,5S,6S,8aR)-5-(2,5-Dimethoxy-3-methyl-benzyl)-2-isopropylidene-5,6,8a-trimethyl-decahydro-naphthalen-1-yl]-propan-1-ol

Base Information

Chemical Name:3-[(1S,4aR,5S,6S,8aR)-5-(2,5-Dimethoxy-3-methyl-benzyl)-2-isopropylidene-5,6,8a-trimethyl-decahydro-naphthalen-1-yl]-propan-1-ol
CAS No.:82471-01-0
Molecular Formula:C₂₉H₄₆O₃
Molecular Weight:442.682
Hs Code.:

Synonyms:3-[(1S,4aR,5S,6S,8aR)-5-(2,5-Dimethoxy-3-methyl-benzyl)-2-isopropylidene-5,6,8a-trimethyl-decahydro-naphthalen-1-yl]-propan-1-ol

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Chemical Property of 3-[(1S,4aR,5S,6S,8aR)-5-(2,5-Dimethoxy-3-methyl-benzyl)-2-isopropylidene-5,6,8a-trimethyl-decahydro-naphthalen-1-yl]-propan-1-ol

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Technology Process of 3-[(1S,4aR,5S,6S,8aR)-5-(2,5-Dimethoxy-3-methyl-benzyl)-2-isopropylidene-5,6,8a-trimethyl-decahydro-naphthalen-1-yl]-propan-1-ol

There total 3 articles about 3-[(1S,4aR,5S,6S,8aR)-5-(2,5-Dimethoxy-3-methyl-benzyl)-2-isopropylidene-5,6,8a-trimethyl-decahydro-naphthalen-1-yl]-propan-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 82471-00-9
3-[(1S,4aR,5S,6S,8aR)-5-(2,5-Dimethoxy-3-methyl-benzyl)-2-isopropylidene-5,6,8a-trimethyl-decahydro-naphthalen-1-yl]-propionic acid methyl ester

: 82471-01-0
3-[(1S,4aR,5S,6S,8aR)-5-(2,5-Dimethoxy-3-methyl-benzyl)-2-isopropylidene-5,6,8a-trimethyl-decahydro-naphthalen-1-yl]-propan-1-ol

Guidance literature:: With lithium aluminium tetrahydride; In diethyl ether; at 0 ℃; for 3h;
DOI:10.1016/0040-4020(82)80215-9

Reference yield:

: 55907-34-1
atomaric acid

: 82471-01-0
3-[(1S,4aR,5S,6S,8aR)-5-(2,5-Dimethoxy-3-methyl-benzyl)-2-isopropylidene-5,6,8a-trimethyl-decahydro-naphthalen-1-yl]-propan-1-ol

Guidance literature:: Multi-step reaction with 3 steps

1: diethyl ether / Ambient temperature

2: 98 percent / anhydrous K₂CO₃ / acetone / 20 h / Heating

3: 94 percent / LiAlH₄ / diethyl ether / 3 h / 0 °C

With lithium aluminium tetrahydride; potassium carbonate; In diethyl ether; acetone;
DOI:10.1016/0040-4020(82)80215-9

Reference yield:

: 82470-99-3
atomaric acid methyl ester

: 82471-01-0
3-[(1S,4aR,5S,6S,8aR)-5-(2,5-Dimethoxy-3-methyl-benzyl)-2-isopropylidene-5,6,8a-trimethyl-decahydro-naphthalen-1-yl]-propan-1-ol

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / anhydrous K₂CO₃ / acetone / 20 h / Heating

2: 94 percent / LiAlH₄ / diethyl ether / 3 h / 0 °C

With lithium aluminium tetrahydride; potassium carbonate; In diethyl ether; acetone;
DOI:10.1016/0040-4020(82)80215-9