tri-O-methyl N-(all-trans-retinoyl)-L-aspartyl-L-aspartate

Base Information

• Chemical Name: tri-O-methyl N-(all-trans-retinoyl)-L-aspartyl-L-aspartate
• CAS No.: 1170316-15-0
• Molecular Formula: C₃₁H₄₄N₂O₈
• Molecular Weight: 572.699
• Mol file: 1170316-15-0.mol

Synonyms:tri-O-methyl N-(all-trans-retinoyl)-L-aspartyl-L-aspartate

Chemical Property of tri-O-methyl N-(all-trans-retinoyl)-L-aspartyl-L-aspartate

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of tri-O-methyl N-(all-trans-retinoyl)-L-aspartyl-L-aspartate

There total 1 articles about tri-O-methyl N-(all-trans-retinoyl)-L-aspartyl-L-aspartate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

N-(all-trans-Retinoyloxy)-succinimide (65646-64-2) + trimethyl L-aspartyl-L-aspartate trifluoroacetate (1170316-09-2) → tri-O-methyl N-(all-trans-retinoyl)-L-aspartyl-L-aspartate (1170316-15-0)

Guidance literature:

trimethyl L-aspartyl-L-aspartate trifluoroacetate; With N-ethyl-N,N-diisopropylamine; In chloroform; Inert atmosphere; Darkness; Cooling with ice;

N-(all-trans-Retinoyloxy)-succinimide; In chloroform; at 20 ℃; Inert atmosphere; Darkness; Cooling with ice;

DOI:10.1016/j.ejmech.2009.03.029

Reference yield: 57.0%

tri-O-methyl N-(all-trans-retinoyl)-L-aspartyl-L-aspartate (1170316-15-0) → N-(all-trans-retinoyl)aspartyl-aspartic acid (1170315-83-9)

Guidance literature:

tri-O-methyl N-(all-trans-retinoyl)-L-aspartyl-L-aspartate; With water; sodium hydroxide; In methanol; at 20 ℃; for 1h; Inert atmosphere; Darkness;

With hydrogenchloride; In methanol; water; at 0 - 40 ℃; pH=3.5 - 7; Darkness;

DOI:10.1016/j.ejmech.2009.03.029

upstream raw materials:

N-(all-trans-Retinoyloxy)-succinimide

trimethyl L-aspartyl-L-aspartate trifluoroacetate

Downstream raw materials:

N-(all-trans-retinoyl)aspartyl-aspartic acid