C₂₇H₂₃ClN₂O₄S

Base Information

Chemical Name:C₂₇H₂₃ClN₂O₄S
CAS No.:1423684-08-5
Molecular Formula:C₂₇H₂₃ClN₂O₄S
Molecular Weight:507.01
Hs Code.:

C<sub>27</sub>H<sub>23</sub>ClN<sub>2</sub>O<sub>4</sub>S

Synonyms:C₂₇H₂₃ClN₂O₄S

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Chemical Property of C₂₇H₂₃ClN₂O₄S

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Technology Process of C₂₇H₂₃ClN₂O₄S

There total 11 articles about C₂₇H₂₃ClN₂O₄S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.7%

: 1423689-72-8
C₂₈H₂₅ClN₂O₄S

: 1423684-08-5
C₂₇H₂₃ClN₂O₄S

Guidance literature:: C₂₈H₂₅ClN₂O₄S; With lithium hydroxide monohydrate; water; In tetrahydrofuran; at 20 ℃;

With hydrogenchloride; In water; at 0 ℃; pH=5.0;

Reference yield:

: 2142-68-9
1-(2-chlorophenyl)ethanone

: 1423684-08-5
C₂₇H₂₃ClN₂O₄S

Guidance literature:: Multi-step reaction with 3 steps

1.1: (S)-tetrahydro-1-butyl-3,3-diphenyl-1H,3H-pyrrolo{2,1-c}{1,3,2}oxazaborole; dimethylsulfide borane complex / tetrahydrofuran / 0.5 h / 20 °C

2.1: diphenyl phosphoryl azide; triethylamine / toluene / 3 h / 80 °C

3.1: water; lithium hydroxide monohydrate / tetrahydrofuran / 20 °C

3.2: 0 °C / pH 5.0

With lithium hydroxide monohydrate; dimethylsulfide borane complex; diphenyl phosphoryl azide; water; triethylamine; (S)-tetrahydro-1-butyl-3,3-diphenyl-1H,3H-pyrrolo{2,1-c}{1,3,2}oxazaborole; In tetrahydrofuran; toluene;

Reference yield:

: 25062-46-8,40979-16-6,34158-73-1
4-bromobenzaldehyde oxime

: 1423684-08-5
C₂₇H₂₃ClN₂O₄S

Guidance literature:: Multi-step reaction with 9 steps

1.1: N-chloro-succinimide / N,N-dimethyl-formamide / 2 h / 15 - 20 °C

2.1: sodium methylate / methanol / 0.67 h / 0 - 25 °C

3.1: potassium phosphate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / water; 1,2-dimethoxyethane / 5 h / 80 °C

4.1: hydrogen / ethanol / 3 h / 20 °C

5.1: Lawessons reagent / dichloromethane / 20 °C

5.2: 24 h

6.1: sodium hydroxide / methanol; tetrahydrofuran / 20 °C

6.2: 0 °C / pH 4.0

7.1: chloro-trimethyl-silane / methanol / 3 h / 0 - 20 °C

8.1: diphenyl phosphoryl azide; triethylamine / toluene / 3 h / 80 °C

9.1: water; lithium hydroxide monohydrate / tetrahydrofuran / 20 °C

9.2: 0 °C / pH 5.0

With Lawessons reagent; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium phosphate; N-chloro-succinimide; chloro-trimethyl-silane; lithium hydroxide monohydrate; diphenyl phosphoryl azide; water; hydrogen; sodium methylate; triethylamine; sodium hydroxide; In tetrahydrofuran; methanol; 1,2-dimethoxyethane; ethanol; dichloromethane; water; N,N-dimethyl-formamide; toluene;