N-(4-isothiocyanato-2-hydroxyphenyl)-2-[(triphenylmethylthio)methylcarbonylamino]ethanamide

Base Information

Chemical Name:N-(4-isothiocyanato-2-hydroxyphenyl)-2-[(triphenylmethylthio)methylcarbonylamino]ethanamide
CAS No.:887268-80-6
Molecular Formula:C₃₀H₂₅N₃O₃S₂
Molecular Weight:539.679
Hs Code.:

Synonyms:N-(4-isothiocyanato-2-hydroxyphenyl)-2-[(triphenylmethylthio)methylcarbonylamino]ethanamide

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Chemical Property of N-(4-isothiocyanato-2-hydroxyphenyl)-2-[(triphenylmethylthio)methylcarbonylamino]ethanamide

Chemical Property:

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Technology Process of N-(4-isothiocyanato-2-hydroxyphenyl)-2-[(triphenylmethylthio)methylcarbonylamino]ethanamide

There total 6 articles about N-(4-isothiocyanato-2-hydroxyphenyl)-2-[(triphenylmethylthio)methylcarbonylamino]ethanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 887268-77-1
N-(5-amino-2-hydroxyphenyl)-2-[(triphenylmethylthio)methylcarbonylamino]ethanamide

: 463-71-8
thiophosgene

: 887268-80-6
N-(4-isothiocyanato-2-hydroxyphenyl)-2-[(triphenylmethylthio)methylcarbonylamino]ethanamide

Guidance literature:: In tetrahydrofuran; at 20 ℃; for 1h; Inert atmosphere;
DOI:10.1016/j.ejmech.2009.09.043

Reference yield:

: 99-57-0
2-hydroxy-5-nitroaniline

: 887268-80-6
N-(4-isothiocyanato-2-hydroxyphenyl)-2-[(triphenylmethylthio)methylcarbonylamino]ethanamide

Guidance literature:: Multi-step reaction with 4 steps

1: 44 percent / dicyclohexylcarbodiimide / tetrahydrofuran / 20 °C

2: 95 percent / hydrogen / Pd/C / methanol / atmospheric pressure

3: 55 percent / triethylamine / acetonitrile / 5 h / 40 °C

4: 87 percent / tetrahydrofuran / 1 h / 20 °C

With hydrogen; triethylamine; dicyclohexyl-carbodiimide; palladium on activated charcoal; In tetrahydrofuran; methanol; acetonitrile;
DOI:10.1002/ejoc.200500810

Reference yield:

: 887268-74-8
N-(2-hydroxy-5-nitrophenyl)-2-[(phenylmethoxy)carbonylamino]ethanamide

: 887268-80-6
N-(4-isothiocyanato-2-hydroxyphenyl)-2-[(triphenylmethylthio)methylcarbonylamino]ethanamide

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / hydrogen / Pd/C / methanol / atmospheric pressure

2: 55 percent / triethylamine / acetonitrile / 5 h / 40 °C

3: 87 percent / tetrahydrofuran / 1 h / 20 °C

With hydrogen; triethylamine; palladium on activated charcoal; In tetrahydrofuran; methanol; acetonitrile;
DOI:10.1002/ejoc.200500810