(1R,2S)-2-<3',4'-(methylenedioxy)benzoyl>-4-cyclohexenyl-N-tosylamide

Base Information

Chemical Name:(1R*,2S*)-2-<3',4'-(methylenedioxy)benzoyl>-4-cyclohexenyl-N-tosylamide
CAS No.:139025-42-6
Molecular Formula:C₂₁H₂₁NO₅S
Molecular Weight:399.467
Hs Code.:

Synonyms:(1R*,2S*)-2-<3',4'-(methylenedioxy)benzoyl>-4-cyclohexenyl-N-tosylamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1R*,2S*)-2-<3',4'-(methylenedioxy)benzoyl>-4-cyclohexenyl-N-tosylamide

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Technology Process of (1R*,2S*)-2-<3',4'-(methylenedioxy)benzoyl>-4-cyclohexenyl-N-tosylamide

There total 8 articles about (1R*,2S*)-2-<3',4'-(methylenedioxy)benzoyl>-4-cyclohexenyl-N-tosylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 17680-04-5
(3,4-methylenedioxy)phenylmagnesium bromide

: 139025-42-6
(1R*,2S*)-2-<3',4'-(methylenedioxy)benzoyl>-4-cyclohexenyl-N-tosylamide

Guidance literature:: Multi-step reaction with 5 steps

1: 95.6 percent / tetrahydrofuran / 0.17 h / ice-cooling

2: 1) Et₃N, ethyl chloroformate, 2) NaN₃ / 1) acetone, ice-cooling, 0.5 h, 2) acetone, water, ice-cooling, 1 h

3: 16 h / Heating

4: trifluoroacetic acid / CH₂Cl₂ / 1 h / Ambient temperature

5: Et₃N / CHCl₃ / 1 h / Ambient temperature

With sodium azide; chloroformic acid ethyl ester; triethylamine; trifluoroacetic acid; In tetrahydrofuran; dichloromethane; chloroform;
DOI:10.1021/jo00052a051

Reference yield:

: 139025-41-5
(1R*,2S*)-2-<3',4'-(methylenedioxy)benzoyl>-4-cyclohexenecarboxylic acid

: 139025-42-6
(1R*,2S*)-2-<3',4'-(methylenedioxy)benzoyl>-4-cyclohexenyl-N-tosylamide

Guidance literature:: Multi-step reaction with 4 steps

1: 1) Et₃N, ethyl chloroformate, 2) NaN₃ / 1) acetone, ice-cooling, 0.5 h, 2) acetone, water, ice-cooling, 1 h

2: 16 h / Heating

3: trifluoroacetic acid / CH₂Cl₂ / 1 h / Ambient temperature

4: Et₃N / CHCl₃ / 1 h / Ambient temperature

With sodium azide; chloroformic acid ethyl ester; triethylamine; trifluoroacetic acid; In dichloromethane; chloroform;
DOI:10.1021/jo00052a051

Reference yield:

: (1R,6S)-6-(Benzo[1,3]dioxole-5-carbonyl)-cyclohex-3-enecarbonyl azide

: 139025-42-6
(1R*,2S*)-2-<3',4'-(methylenedioxy)benzoyl>-4-cyclohexenyl-N-tosylamide

Guidance literature:: Multi-step reaction with 3 steps

1: 16 h / Heating

2: trifluoroacetic acid / CH₂Cl₂ / 1 h / Ambient temperature

3: Et₃N / CHCl₃ / 1 h / Ambient temperature

With triethylamine; trifluoroacetic acid; In dichloromethane; chloroform;
DOI:10.1021/jo00052a051