2-[(bis-pyridin-2-ylmethylamino)methyl]-5-nitrobenzoic acid methyl ester

Base Information

Chemical Name:2-[(bis-pyridin-2-ylmethylamino)methyl]-5-nitrobenzoic acid methyl ester
CAS No.:1574531-88-6
Molecular Formula:C₂₁H₂₀N₄O₄
Molecular Weight:392.414
Hs Code.:

Synonyms:2-[(bis-pyridin-2-ylmethylamino)methyl]-5-nitrobenzoic acid methyl ester

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Chemical Property of 2-[(bis-pyridin-2-ylmethylamino)methyl]-5-nitrobenzoic acid methyl ester

Chemical Property:

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Technology Process of 2-[(bis-pyridin-2-ylmethylamino)methyl]-5-nitrobenzoic acid methyl ester

There total 4 articles about 2-[(bis-pyridin-2-ylmethylamino)methyl]-5-nitrobenzoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 90725-68-1
methyl 2-(bromomethyl)-5-nitrobenzoate

: 1539-42-0
bis[(2-pyridyl)methyl]amine

: 1574531-88-6
2-[(bis-pyridin-2-ylmethylamino)methyl]-5-nitrobenzoic acid methyl ester

Guidance literature:: With triethylamine; In tetrahydrofuran; for 7h; Reflux;
DOI:10.1021/ic402695c

Reference yield:

: 89-71-4
2-Methyl-benzoic acid methyl ester

: 1574531-88-6
2-[(bis-pyridin-2-ylmethylamino)methyl]-5-nitrobenzoic acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: sulfuric acid; nitric acid

2: N-Bromosuccinimide; dibenzoyl peroxide; tetrachloromethane

3: triethylamine / tetrahydrofuran / 7 h / Reflux

With tetrachloromethane; N-Bromosuccinimide; sulfuric acid; nitric acid; triethylamine; dibenzoyl peroxide; In tetrahydrofuran;
DOI:10.1021/ic402695c

Reference yield:

: 118-90-1
ortho-methylbenzoic acid

: 1574531-88-6
2-[(bis-pyridin-2-ylmethylamino)methyl]-5-nitrobenzoic acid methyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: sulfuric acid

2: sulfuric acid; nitric acid

3: N-Bromosuccinimide; dibenzoyl peroxide; tetrachloromethane

4: triethylamine / tetrahydrofuran / 7 h / Reflux

With tetrachloromethane; N-Bromosuccinimide; sulfuric acid; nitric acid; triethylamine; dibenzoyl peroxide; In tetrahydrofuran;
DOI:10.1021/ic402695c