12-(3-phenylpropyl)-8,9-dihydro[1,4]benzodioxino[6,7-g]pteridine-2,4(3H,12H)-dione

Base Information

Chemical Name:12-(3-phenylpropyl)-8,9-dihydro[1,4]benzodioxino[6,7-g]pteridine-2,4(3H,12H)-dione
CAS No.:1338684-45-9
Molecular Formula:C₂₁H₁₈N₄O₄
Molecular Weight:390.398
Hs Code.:

Synonyms:12-(3-phenylpropyl)-8,9-dihydro[1,4]benzodioxino[6,7-g]pteridine-2,4(3H,12H)-dione

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Chemical Property of 12-(3-phenylpropyl)-8,9-dihydro[1,4]benzodioxino[6,7-g]pteridine-2,4(3H,12H)-dione

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Technology Process of 12-(3-phenylpropyl)-8,9-dihydro[1,4]benzodioxino[6,7-g]pteridine-2,4(3H,12H)-dione

There total 4 articles about 12-(3-phenylpropyl)-8,9-dihydro[1,4]benzodioxino[6,7-g]pteridine-2,4(3H,12H)-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

: 61066-33-9,61066-34-0,61066-35-1,61127-23-9
pyrimidine-2,4,5,6(1H,3H)-tetraone

: 1178618-47-7
N-(3-phenylpropyl)-2,3-dihydro-1,4-benzodioxine-6,7-diamine

: 1338684-45-9
12-(3-phenylpropyl)-8,9-dihydro[1,4]benzodioxino[6,7-g]pteridine-2,4(3H,12H)-dione

Guidance literature:: With boric acid; acetic acid; at 20 ℃; for 18h;

Reference yield:

: 637-59-2
1-Bromo-3-phenylpropane

: 1338684-45-9
12-(3-phenylpropyl)-8,9-dihydro[1,4]benzodioxino[6,7-g]pteridine-2,4(3H,12H)-dione

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.75 h / 0 - 20 °C

1.2: 18 h / 20 °C

2.1: hydrogen / ethanol / 24 h / 20 °C / 760.05 Torr

3.1: boric acid; acetic acid / 18 h / 20 °C

With hydrogen; boric acid; sodium hydride; acetic acid; In ethanol; N,N-dimethyl-formamide; mineral oil;

Reference yield:

: 62140-78-7
7-nitro-2,3-dihydro-1,4-benzodioxin-6-amine

: 1338684-45-9
12-(3-phenylpropyl)-8,9-dihydro[1,4]benzodioxino[6,7-g]pteridine-2,4(3H,12H)-dione

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.75 h / 0 - 20 °C

1.2: 18 h / 20 °C

2.1: hydrogen / ethanol / 24 h / 20 °C / 760.05 Torr

3.1: boric acid; acetic acid / 18 h / 20 °C

With hydrogen; boric acid; sodium hydride; acetic acid; In ethanol; N,N-dimethyl-formamide; mineral oil;