3-(4-chlorophenyl)imino-2-(4-methoxy-2-methylphenylimino)-2,3-dihydrobenzofuran

Base Information

• Chemical Name: 3-(4-chlorophenyl)imino-2-(4-methoxy-2-methylphenylimino)-2,3-dihydrobenzofuran
• CAS No.: 1224234-81-4
• Molecular Formula: C₂₂H₁₇ClN₂O₂
• Molecular Weight: 376.842

Synonyms:3-(4-chlorophenyl)imino-2-(4-methoxy-2-methylphenylimino)-2,3-dihydrobenzofuran

Chemical Property of 3-(4-chlorophenyl)imino-2-(4-methoxy-2-methylphenylimino)-2,3-dihydrobenzofuran

Chemical Property:

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Technology Process of 3-(4-chlorophenyl)imino-2-(4-methoxy-2-methylphenylimino)-2,3-dihydrobenzofuran

There total 2 articles about 3-(4-chlorophenyl)imino-2-(4-methoxy-2-methylphenylimino)-2,3-dihydrobenzofuran which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

N-(4-chlorophenyl)salicylaldimine (782-77-4,82306-73-8) + 1-isocyano-4-methoxy-2-methylbenzene (1930-89-8) → 3-(4-chlorophenyl)imino-2-(4-methoxy-2-methylphenylimino)-2,3-dihydrobenzofuran (1224234-81-4)

Guidance literature:

N-(4-chlorophenyl)salicylaldimine; 1-isocyano-4-methoxy-2-methylbenzene; With boron trifluoride diethyl etherate; In dichloromethane; at 0 ℃;

In diethyl ether; hexane; at 20 ℃;

DOI:10.1055/s-0029-1218609

Reference yield:

N-(4-chlorophenyl)salicylaldimine (782-77-4,82306-73-8) + 1-isocyano-4-methoxy-2-methylbenzene (1930-89-8) → 3-(4-chlorophenyl)imino-2-(4-methoxy-2-methylphenylimino)-2,3-dihydrobenzofuran (1224234-81-4) + C22H19ClN2O2

Guidance literature:

With boron trifluoride diethyl etherate; In dichloromethane; at 0 ℃;

DOI:10.1055/s-0029-1218609

upstream raw materials:

N-(4-chlorophenyl)salicylaldimine

1-isocyano-4-methoxy-2-methylbenzene

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