{Tc(SC(NH₂)2)6}⁽³⁺⁾*3Cl^(1-)={Tc(SC(NH₂)2)6}Cl₃

Base Information

Chemical Name:{Tc(SC(NH₂)2)6}⁽³⁺⁾*3Cl^(1-)={Tc(SC(NH₂)2)6}Cl₃
CAS No.:89172-46-3
Molecular Formula:C₆H₂₄N₁₂S₆Tc*3Cl
Molecular Weight:660.999
Hs Code.:

{Tc(SC(NH<sub>2</sub>)2)6}<sup>(3+)</sup>*3Cl<sup>(1-)</sup>={Tc(SC(NH<sub>2</sub>)2)6}Cl<sub>3</sub>

Synonyms:{Tc(SC(NH₂)2)6}⁽³⁺⁾*3Cl^(1-)={Tc(SC(NH₂)2)6}Cl₃

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Chemical Property of {Tc(SC(NH₂)2)6}⁽³⁺⁾*3Cl^(1-)={Tc(SC(NH₂)2)6}Cl₃

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Technology Process of {Tc(SC(NH₂)2)6}⁽³⁺⁾*3Cl^(1-)={Tc(SC(NH₂)2)6}Cl₃

There total 1 articles about {Tc(SC(NH₂)2)6}⁽³⁺⁾*3Cl^(1-)={Tc(SC(NH₂)2)6}Cl₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 34035-97-7
ammonium pertechnetate

: 17356-08-0
thiourea

: 89172-46-3
{Tc(SC(NH₂)2)6}⁽³⁺⁾*3Cl^(1-)={Tc(SC(NH₂)2)6}Cl₃

Guidance literature:: With hydrogenchloride; In ethanol; 0.469 M NH4TcO4 was added to stirred soln. of thiourea in EtOH containing 12 N HCl, 2 h; filtered by suction, washed with cold EtOH, dried in vac.; elem. anal.;

Reference yield: 33.0%

: 89172-46-3
{Tc(SC(NH₂)2)6}⁽³⁺⁾*3Cl^(1-)={Tc(SC(NH₂)2)6}Cl₃

: 1663-45-2
1,2-bis-(diphenylphosphino)ethane

: dichlorobis(1,2-bis(diphenylphosphino)ethane)technetium(III) chloride dihydrate

Guidance literature:: With hydrogenchloride; In methanol; diphos was added to stirred soln. of Tc-complex (molar ratio 4.7:1) in MeOH containing 12 N HCl, refluxed for 1 h; cooled to room temp., solvent removed in vac., filtered, 12 N HCl addedto filtrate, stood at 5°C for 48 h, filtered by suction, washed with ether-EtOH, dried in vac.; elem. anal.;