Technology Process of C20H30N4O12S
There total 9 articles about C20H30N4O12S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C28H38N4O16S;
With
sodium methylate;
In
methanol;
at 20 ℃;
for 12h;
Inert atmosphere;
pH=7;
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: dmap / dichloromethane / 12 h / 20 °C
2.1: dichloromethane / 0.17 h / 20 °C / Inert atmosphere
3.1: N,N-dimethyl-formamide / 2 h / 20 °C / Inert atmosphere
4.1: dmap / dichloromethane / 12 h / 20 °C
5.1: triethylamine / dichloromethane / 12 h / 20 °C / Inert atmosphere
6.1: trifluoroacetic acid / dichloromethane / 0 °C / Inert atmosphere
7.1: sodium methylate / methanol / 12 h / 20 °C / Inert atmosphere
7.2: H+/Na+ ion-exchange resin / pH 7
With
dmap; sodium methylate; triethylamine; trifluoroacetic acid;
In
methanol; dichloromethane; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 9 steps
1.1: silver(l) oxide / acetonitrile / 12 h / 20 °C / Darkness; Inert atmosphere
2.1: sodium tetrahydroborate / isopropyl alcohol; chloroform / 12 h / 0 - 20 °C / Inert atmosphere
3.1: dmap / dichloromethane / 12 h / 20 °C
4.1: dichloromethane / 0.17 h / 20 °C / Inert atmosphere
5.1: N,N-dimethyl-formamide / 2 h / 20 °C / Inert atmosphere
6.1: dmap / dichloromethane / 12 h / 20 °C
7.1: triethylamine / dichloromethane / 12 h / 20 °C / Inert atmosphere
8.1: trifluoroacetic acid / dichloromethane / 0 °C / Inert atmosphere
9.1: sodium methylate / methanol / 12 h / 20 °C / Inert atmosphere
9.2: H+/Na+ ion-exchange resin / pH 7
With
dmap; sodium tetrahydroborate; sodium methylate; triethylamine; trifluoroacetic acid; silver(l) oxide;
In
methanol; dichloromethane; chloroform; N,N-dimethyl-formamide; isopropyl alcohol; acetonitrile;