trans-(E/Z)-4-(hydroxyimino-methyl)-cyclohexanecarboxylic acid methyl ester

Base Information

Chemical Name:trans-(E/Z)-4-(hydroxyimino-methyl)-cyclohexanecarboxylic acid methyl ester
CAS No.:1346450-07-4
Molecular Formula:C₉H₁₅NO₃
Molecular Weight:185.223
Hs Code.:

Synonyms:trans-(E/Z)-4-(hydroxyimino-methyl)-cyclohexanecarboxylic acid methyl ester

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Chemical Property of trans-(E/Z)-4-(hydroxyimino-methyl)-cyclohexanecarboxylic acid methyl ester

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Technology Process of trans-(E/Z)-4-(hydroxyimino-methyl)-cyclohexanecarboxylic acid methyl ester

There total 4 articles about trans-(E/Z)-4-(hydroxyimino-methyl)-cyclohexanecarboxylic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 54274-80-5
trans-4-formyl-cyclohexanecarboxylic acid methyl ester

: 1346450-07-4
trans-(E/Z)-4-(hydroxyimino-methyl)-cyclohexanecarboxylic acid methyl ester

Guidance literature:: With hydroxylamine hydrochloride; sodium acetate; In methanol; at 0 - 5 ℃; for 20h;

Reference yield:

: ethyl acetamidate hydrochloride

: trans-methyl 4-(chloro(hydroxyimino)methyl)cyclohexanecarboxylate

: trans-4-(5-methyl-[1,2,4]oxadiazol-3-yl)-cyclohexanecarboxylic acid methyl ester

: 1346450-07-4
trans-(E/Z)-4-(hydroxyimino-methyl)-cyclohexanecarboxylic acid methyl ester

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 5 ℃;

Reference yield:

: 15177-67-0
trans-4-(methoxycarbonyl)cyclohexanecarboxylic acid

: 1346450-07-4
trans-(E/Z)-4-(hydroxyimino-methyl)-cyclohexanecarboxylic acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: dimethylsulfide borane complex / tetrahydrofuran / 4.25 h / 0 °C

2.1: dimethyl sulfoxide; oxalyl dichloride / dichloromethane / 0.5 h / -65 °C

2.2: 0.25 h / -65 °C

3.1: sodium acetate; hydroxylamine hydrochloride / methanol / 20 h / 0 - 5 °C

With oxalyl dichloride; dimethylsulfide borane complex; hydroxylamine hydrochloride; sodium acetate; dimethyl sulfoxide; In tetrahydrofuran; methanol; dichloromethane;