C₂₉H₃₈N₂O₇

Base Information

Chemical Name:C₂₉H₃₈N₂O₇
CAS No.:1609453-88-4
Molecular Formula:C₂₉H₃₈N₂O₇
Molecular Weight:526.63
Hs Code.:

C<sub>29</sub>H<sub>38</sub>N<sub>2</sub>O<sub>7</sub>

Synonyms:C₂₉H₃₈N₂O₇

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Chemical Property of C₂₉H₃₈N₂O₇

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Technology Process of C₂₉H₃₈N₂O₇

There total 7 articles about C₂₉H₃₈N₂O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1609453-84-0
C₂₃H₂₇NO₆

: 6306-52-1
L-valine methylester hydrochloride

: 1609453-88-4
C₂₉H₃₈N₂O₇

Guidance literature:: C₂₃H₂₇NO₆; L-valine methylester hydrochloride; With sodium sulfate; N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 0.166667h; Inert atmosphere;

With titanium(IV) isopropylate; In dichloromethane; at 20 ℃; Inert atmosphere;
DOI:10.1021/jo500493c

Reference yield:

: 90-96-0
bis(p-methoxyphenyl)methanone

: 1609453-88-4
C₂₉H₃₈N₂O₇

Guidance literature:: Multi-step reaction with 6 steps

1.1: sulfuric acid / methanol / 30 h / 20 °C / Inert atmosphere

2.1: (1S)-10-camphorsulfonic acid / toluene / 5 h / Reflux; Inert atmosphere

3.1: lithium hydroxide monohydrate; water / tetrahydrofuran / 20 °C / Inert atmosphere

4.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / dichloromethane / 2 h / 20 °C / Inert atmosphere

4.2: 20 °C / Inert atmosphere

5.1: lithium aluminium tetrahydride / tetrahydrofuran / 0.2 h / 20 °C / Inert atmosphere

6.1: N-ethyl-N,N-diisopropylamine; sodium sulfate / dichloromethane / 0.17 h / 20 °C / Inert atmosphere

6.2: 20 °C / Inert atmosphere

With lithium aluminium tetrahydride; lithium hydroxide monohydrate; sulfuric acid; (1S)-10-camphorsulfonic acid; water; benzotriazol-1-ol; sodium sulfate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; methanol; dichloromethane; toluene;
DOI:10.1021/jo500493c

Reference yield:

: 95715-85-8
2-(tert-butoxycarbonylamino)-3-hydroxypropionic acid methyl ester

: 1609453-88-4
C₂₉H₃₈N₂O₇

Guidance literature:: Multi-step reaction with 5 steps

1.1: (1S)-10-camphorsulfonic acid / toluene / 5 h / Reflux; Inert atmosphere

2.1: lithium hydroxide monohydrate; water / tetrahydrofuran / 20 °C / Inert atmosphere

3.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / dichloromethane / 2 h / 20 °C / Inert atmosphere

3.2: 20 °C / Inert atmosphere

4.1: lithium aluminium tetrahydride / tetrahydrofuran / 0.2 h / 20 °C / Inert atmosphere

5.1: N-ethyl-N,N-diisopropylamine; sodium sulfate / dichloromethane / 0.17 h / 20 °C / Inert atmosphere

5.2: 20 °C / Inert atmosphere

With lithium aluminium tetrahydride; lithium hydroxide monohydrate; (1S)-10-camphorsulfonic acid; water; benzotriazol-1-ol; sodium sulfate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane; toluene;
DOI:10.1021/jo500493c