dimethyl exo,exo-2,4-diphenyl-9,10-diazatetracyclo[3.3.2.0^2.4.0^6.8]dec-9-ene-1,5-dicarboxylate

Base Information

• Chemical Name: dimethyl exo,exo-2,4-diphenyl-9,10-diazatetracyclo[3.3.2.0^2.4.0^6.8]dec-9-ene-1,5-dicarboxylate
• CAS No.: 69901-14-0
• Molecular Formula: C₂₄H₂₂N₂O₄
• Molecular Weight: 402.45

Synonyms:dimethyl exo,exo-2,4-diphenyl-9,10-diazatetracyclo[3.3.2.0^2.4.0^6.8]dec-9-ene-1,5-dicarboxylate

Chemical Property of dimethyl exo,exo-2,4-diphenyl-9,10-diazatetracyclo[3.3.2.0^2.4.0^6.8]dec-9-ene-1,5-dicarboxylate

Chemical Property:

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Technology Process of dimethyl exo,exo-2,4-diphenyl-9,10-diazatetracyclo[3.3.2.0^2.4.0^6.8]dec-9-ene-1,5-dicarboxylate

There total 2 articles about dimethyl exo,exo-2,4-diphenyl-9,10-diazatetracyclo[3.3.2.0^2.4.0^6.8]dec-9-ene-1,5-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

1,2-Diphenylcyclopropen (24168-52-3) + Diazanorcaradien (27666-78-0) → dimethyl exo,exo-2,4-diphenyl-9,10-diazatetracyclo[3.3.2.02.4.06.8]dec-9-ene-1,5-dicarboxylate (69901-14-0)

Guidance literature:

In dichloromethane; for 40h; Heating;

DOI:10.1002/1099-0690(200107)2001:14<2639::aid-ejoc2639>3.0.co;2-0

Reference yield:

→ 2,4-diphenyl-9,10-diaza-tetracyclo[3.3.2.02,4.06,8]dec-9-ene-1,5-dicarboxylic acid dimethyl ester (69901-14-0)

Guidance literature:

Tetrazincarbonester 1, Diphenylcyclopropen 2;

DOI:10.1016/S0040-4039(01)95093-2

Reference yield: 98.0%

dimethyl exo,exo-2,4-diphenyl-9,10-diazatetracyclo[3.3.2.02.4.06.8]dec-9-ene-1,5-dicarboxylate (69901-14-0) → C22H18N2O4

Guidance literature:

With potassium hydroxide; In methanol;

DOI:10.1002/1099-0690(200107)2001:14<2639::aid-ejoc2639>3.0.co;2-0

upstream raw materials:

1,2-Diphenylcyclopropen

Diazanorcaradien

Downstream raw materials:

exo,exo-2,4-diphenyl-9,10-diazatetracyclo[3.3.2.0^2.4.0^6.8]dec-9-ene-1,5-dicarbonitrile

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