5-Hexen-2-ol, 2-(4-methylbenzenesulfonate)

Base Information

Chemical Name:5-Hexen-2-ol, 2-(4-methylbenzenesulfonate)
CAS No.:171557-94-1
Molecular Formula:C₁₃H₁₈O₃S
Molecular Weight:254.35
Hs Code.:
DSSTox Substance ID:DTXSID301268535

Synonyms:5-Hexen-2-ol, 2-(4-methylbenzenesulfonate);DTXSID301268535;171557-94-1

Suppliers and Price of 5-Hexen-2-ol, 2-(4-methylbenzenesulfonate)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 0 raw suppliers

Chemical Property of 5-Hexen-2-ol, 2-(4-methylbenzenesulfonate)

Chemical Property:

XLogP3:3.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:6
Exact Mass:254.09766561
Heavy Atom Count:17
Complexity:321

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC1=CC=C(C=C1)S(=O)(=O)OC(C)CCC=C

Technology Process of 5-Hexen-2-ol, 2-(4-methylbenzenesulfonate)

There total 1 articles about 5-Hexen-2-ol, 2-(4-methylbenzenesulfonate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 17397-24-9,17397-29-4,54774-27-5,626-94-8
hex-5-en-2-ol

: 98-59-9
p-toluenesulfonyl chloride

: 171557-94-1
toluene-4-sulfonic acid 1-methylpent-4-enyl ester

Guidance literature:: With pyridine; In dichloromethane; at 0 - 23 ℃; for 16h; Inert atmosphere;
DOI:10.1002/ejoc.202100360

Reference yield: 55.0%

: 171557-94-1
toluene-4-sulfonic acid 1-methylpent-4-enyl ester

: 592-41-6,25067-06-5
1-hexene

Guidance literature:: With lithium aluminium tetrahydride; at 0 - 23 ℃; for 4h;
DOI:10.1002/ejoc.202100360

Reference yield:

: 171557-94-1
toluene-4-sulfonic acid 1-methylpent-4-enyl ester

: 1003-38-9
2,5-dimethyltetrahydrofuran

Guidance literature:: Multi-step reaction with 2 steps

1: 64 percent / dimethylformamide / 14 h

2: naphthalene-2-thiol / benzene-d6 / 0.08 h / 15 °C / Irradiation

With 2-Naphthalenethiol; In benzene-d6; N,N-dimethyl-formamide;
DOI:10.1021/jo00126a021