(2,5-Dimethoxy-3-methyl-phenyl)-(6,8,8-trimethyl-1,4-dithia-spiro[4.5]dec-6-en-7-yl)-methanol

Base Information

Chemical Name:(2,5-Dimethoxy-3-methyl-phenyl)-(6,8,8-trimethyl-1,4-dithia-spiro[4.5]dec-6-en-7-yl)-methanol
CAS No.:108287-50-9
Molecular Formula:C₂₁H₃₀O₃S₂
Molecular Weight:394.599
Hs Code.:

Synonyms:(2,5-Dimethoxy-3-methyl-phenyl)-(6,8,8-trimethyl-1,4-dithia-spiro[4.5]dec-6-en-7-yl)-methanol

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Chemical Property of (2,5-Dimethoxy-3-methyl-phenyl)-(6,8,8-trimethyl-1,4-dithia-spiro[4.5]dec-6-en-7-yl)-methanol

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Technology Process of (2,5-Dimethoxy-3-methyl-phenyl)-(6,8,8-trimethyl-1,4-dithia-spiro[4.5]dec-6-en-7-yl)-methanol

There total 4 articles about (2,5-Dimethoxy-3-methyl-phenyl)-(6,8,8-trimethyl-1,4-dithia-spiro[4.5]dec-6-en-7-yl)-methanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 28120-76-5
methyl 2,6,6-trimethyl-3-oxocyclohex-1-ene-1-carboxylate

: 108287-50-9
(2,5-Dimethoxy-3-methyl-phenyl)-(6,8,8-trimethyl-1,4-dithia-spiro[4.5]dec-6-en-7-yl)-methanol

Guidance literature:: Multi-step reaction with 4 steps

1: 95 percent / BF₃*etherate / CH₂Cl₂ / 30 h / Ambient temperature

2: 90 percent / LiAlH₄ / diethyl ether / 5 h / Heating

3: 90 percent / MnO₂ / benzene / 72 h / Ambient temperature

4: 1.) Mg, iodine, ethylene bromide / 1) THF, reflux, 120 min; 2) THF, Et₂O, 5 h, reflux

With manganese(IV) oxide; lithium aluminium tetrahydride; boron trifluoride diethyl etherate; iodine; magnesium; ethylene dibromide; In diethyl ether; dichloromethane; benzene;

Reference yield:

: 91029-33-3
3,3-ethylenedithio derivative of β-cyclogeraniol

: 108287-50-9
(2,5-Dimethoxy-3-methyl-phenyl)-(6,8,8-trimethyl-1,4-dithia-spiro[4.5]dec-6-en-7-yl)-methanol

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / MnO₂ / benzene / 72 h / Ambient temperature

2: 1.) Mg, iodine, ethylene bromide / 1) THF, reflux, 120 min; 2) THF, Et₂O, 5 h, reflux

With manganese(IV) oxide; iodine; magnesium; ethylene dibromide; In benzene;

Reference yield:

: 91029-32-2
3,3-ethylenedithio derivative of methyl β-cyclogeranate

: 108287-50-9
(2,5-Dimethoxy-3-methyl-phenyl)-(6,8,8-trimethyl-1,4-dithia-spiro[4.5]dec-6-en-7-yl)-methanol

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / LiAlH₄ / diethyl ether / 5 h / Heating

2: 90 percent / MnO₂ / benzene / 72 h / Ambient temperature

3: 1.) Mg, iodine, ethylene bromide / 1) THF, reflux, 120 min; 2) THF, Et₂O, 5 h, reflux

With manganese(IV) oxide; lithium aluminium tetrahydride; iodine; magnesium; ethylene dibromide; In diethyl ether; benzene;