C₄₃H₄₄LuN₅O₂Si

Base Information

• Chemical Name: C₄₃H₄₄LuN₅O₂Si
• CAS No.: 1275613-14-3
• Molecular Formula: C₄₃H₄₄LuN₅O₂Si
• Molecular Weight: 865.907
• Mol file: 1275613-14-3.mol

Synonyms:C₄₃H₄₄LuN₅O₂Si

Chemical Property of C₄₃H₄₄LuN₅O₂Si

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₄₃H₄₄LuN₅O₂Si

There total 3 articles about C₄₃H₄₄LuN₅O₂Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

C43H49N5O2Si → C43H44LuN5O2Si (1275613-14-3)

Guidance literature:

With lutetium(III) acetate tetrahydrate; sodium acetate; In methanol; chloroform; at 20 ℃; for 72h; Darkness;

DOI:10.1016/j.ejmech.2010.12.007

Reference yield:

C23H26N2O4Si (1275576-04-9) → C43H44LuN5O2Si (1275613-14-3)

Guidance literature:

Multi-step reaction with 2 steps

1.1: trifluoroacetic acid / 0.17 h / 20 °C / Inert atmosphere

1.2: 2 h / 20 °C / Inert atmosphere; Darkness

1.3: Cooling with ice

2.1: lutetium(III) acetate tetrahydrate; sodium acetate / methanol; chloroform / 72 h / 20 °C / Darkness

With lutetium(III) acetate tetrahydrate; sodium acetate; trifluoroacetic acid; In methanol; chloroform;

DOI:10.1016/j.ejmech.2010.12.007

Reference yield:

C22H27N3O4 (500003-14-5) → C43H44LuN5O2Si (1275613-14-3)

Guidance literature:

Multi-step reaction with 2 steps

1.1: trifluoroacetic acid / 0.17 h / 20 °C / Inert atmosphere

1.2: 2 h / 20 °C / Inert atmosphere; Darkness

1.3: Cooling with ice

2.1: lutetium(III) acetate tetrahydrate; sodium acetate / methanol; chloroform / 72 h / 20 °C / Darkness

With lutetium(III) acetate tetrahydrate; sodium acetate; trifluoroacetic acid; In methanol; chloroform;

DOI:10.1016/j.ejmech.2010.12.007

upstream raw materials:

C₂₃H₂₆N₂O₄Si

C₂₂H₂₇N₃O₄