C₅₈H₇₇F₃O₇S₂Si₂

Base Information

Chemical Name:C₅₈H₇₇F₃O₇S₂Si₂
CAS No.:1392308-83-6
Molecular Formula:C₅₈H₇₇F₃O₇S₂Si₂
Molecular Weight:1063.54
Hs Code.:

C<sub>58</sub>H<sub>77</sub>F<sub>3</sub>O<sub>7</sub>S<sub>2</sub>Si<sub>2</sub>

Synonyms:C₅₈H₇₇F₃O₇S₂Si₂

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Chemical Property of C₅₈H₇₇F₃O₇S₂Si₂

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Technology Process of C₅₈H₇₇F₃O₇S₂Si₂

There total 10 articles about C₅₈H₇₇F₃O₇S₂Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 1392308-81-4
C₄₈H₇₀O₅S₂Si₂

: 39637-99-5,20445-33-4
(S)-(+)-2-methoxy-2-trifluoromethyl-2-phenylacetyl chloride

: 1392308-83-6
C₅₈H₇₇F₃O₇S₂Si₂

Guidance literature:: With dmap; triethylamine; In dichloromethane; at 0 - 25 ℃; for 0.5h;
DOI:10.1002/anie.201201653

Reference yield:

: 14947-48-9
2-(2'-hydroxyethyl)-1,3-dithiane

: 1392308-83-6
C₅₈H₇₇F₃O₇S₂Si₂

Guidance literature:: Multi-step reaction with 6 steps

1.1: (+)-10-camphorsulfonic acid / dichloromethane / 1 h / 0 °C

2.1: n-butyllithium; dibutylmagnesium / tetrahydrofuran; hexane; n-heptane / 1 h / 25 °C

2.2: 1.5 h / -78 - 0 °C

3.1: zinc(II) chloride / diethyl ether; dichloromethane / 3 h / 25 °C

4.1: sulfur trioxide pyridine complex; dimethyl sulfoxide; N-ethyl-N,N-diisopropylamine / dichloromethane / 1 h / 0 °C

5.1: tert.-butyl lithium / diethyl ether; pentane / 1 h / -78 °C

5.2: 1 h / -78 - 0 °C

6.1: dmap; triethylamine / dichloromethane / 0.5 h / 0 - 25 °C

With dmap; n-butyllithium; dibutylmagnesium; tert.-butyl lithium; sulfur trioxide pyridine complex; dimethyl sulfoxide; (+)-10-camphorsulfonic acid; triethylamine; N-ethyl-N,N-diisopropylamine; zinc(II) chloride; In tetrahydrofuran; diethyl ether; hexane; n-heptane; dichloromethane; pentane; 4.1: Parikh-Doering oxidation;
DOI:10.1002/anie.201201653

Reference yield:

: 5849-13-8
2-(2,2-diethoxyethyl)-1,3-dithiane

: 1392308-83-6
C₅₈H₇₇F₃O₇S₂Si₂

Guidance literature:: Multi-step reaction with 8 steps

1.1: water; toluene-4-sulfonic acid / tetrahydrofuran / 12 h / 45 °C

2.1: sodium tetrahydroborate / ethanol / 3 h / 0 °C

3.1: (+)-10-camphorsulfonic acid / dichloromethane / 1 h / 0 °C

4.1: n-butyllithium; dibutylmagnesium / tetrahydrofuran; hexane; n-heptane / 1 h / 25 °C

4.2: 1.5 h / -78 - 0 °C

5.1: zinc(II) chloride / diethyl ether; dichloromethane / 3 h / 25 °C

6.1: sulfur trioxide pyridine complex; dimethyl sulfoxide; N-ethyl-N,N-diisopropylamine / dichloromethane / 1 h / 0 °C

7.1: tert.-butyl lithium / diethyl ether; pentane / 1 h / -78 °C

7.2: 1 h / -78 - 0 °C

8.1: dmap; triethylamine / dichloromethane / 0.5 h / 0 - 25 °C

With dmap; sodium tetrahydroborate; n-butyllithium; dibutylmagnesium; water; tert.-butyl lithium; sulfur trioxide pyridine complex; toluene-4-sulfonic acid; dimethyl sulfoxide; (+)-10-camphorsulfonic acid; triethylamine; N-ethyl-N,N-diisopropylamine; zinc(II) chloride; In tetrahydrofuran; diethyl ether; ethanol; hexane; n-heptane; dichloromethane; pentane; 6.1: Parikh-Doering oxidation;
DOI:10.1002/anie.201201653