ethyl (E)-3-(3,4-Bis(2-((tert-butyldimethylsilyl)oxy)ethoxy)phenyl)acrylate

Base Information

Chemical Name:ethyl (E)-3-(3,4-Bis(2-((tert-butyldimethylsilyl)oxy)ethoxy)phenyl)acrylate
CAS No.:1609031-14-2
Molecular Formula:C₂₇H₄₈O₆Si₂
Molecular Weight:524.846
Hs Code.:

Synonyms:ethyl (E)-3-(3,4-Bis(2-((tert-butyldimethylsilyl)oxy)ethoxy)phenyl)acrylate

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Chemical Property of ethyl (E)-3-(3,4-Bis(2-((tert-butyldimethylsilyl)oxy)ethoxy)phenyl)acrylate

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Technology Process of ethyl (E)-3-(3,4-Bis(2-((tert-butyldimethylsilyl)oxy)ethoxy)phenyl)acrylate

There total 1 articles about ethyl (E)-3-(3,4-Bis(2-((tert-butyldimethylsilyl)oxy)ethoxy)phenyl)acrylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 74257-25-3,102-37-4,66648-50-8
ethyl caffeate

: 102229-10-7
2-(tert-butyldimethylsilyloxy)ethanol

: 1609031-14-2
ethyl (E)-3-(3,4-Bis(2-((tert-butyldimethylsilyl)oxy)ethoxy)phenyl)acrylate

Guidance literature:: With di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; at 0 ℃; for 36h; Reflux;
DOI:10.1021/jm5000672

Reference yield: 100.0%

: 1609031-14-2
ethyl (E)-3-(3,4-Bis(2-((tert-butyldimethylsilyl)oxy)ethoxy)phenyl)acrylate

: 1609031-15-3
(E)-3-(3,4-bis(2-hydroxyethoxy)phenyl)acrylic Acid

Guidance literature:: ethyl (E)-3-(3,4-Bis(2-((tert-butyldimethylsilyl)oxy)ethoxy)phenyl)acrylate; With sodium hydroxide; In tetrahydrofuran; for 48h; Reflux;

With hydrogenchloride; In tetrahydrofuran; water; pH=4;
DOI:10.1021/jm5000672

Reference yield:

: 1609031-14-2
ethyl (E)-3-(3,4-Bis(2-((tert-butyldimethylsilyl)oxy)ethoxy)phenyl)acrylate

: 1609030-89-8
(E)-3-(3,4-bis(2-hydroxyethoxy)phenyl)-N-(2-(2-methyl-1H-indol-3-yl)ethyl)acrylamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydroxide / tetrahydrofuran / 48 h / Reflux

1.2: pH 4

2.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap / dichloromethane / 8 h / 20 °C

With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; sodium hydroxide; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jm5000672