Technology Process of C30H33ClN2O5
There total 6 articles about C30H33ClN2O5 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
triethylamine;
In
N,N-dimethyl acetamide;
at -15 ℃;
for 1.5h;
Cooling with ice;
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: thionyl chloride / 2 h / Reflux
1.2: 0.17 h / 0 °C
2.1: triethylamine / N,N-dimethyl acetamide / 1.5 h / -15 °C / Cooling with ice
With
thionyl chloride; triethylamine;
In
N,N-dimethyl acetamide;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: potassium carbonate; sodium iodide / N,N-dimethyl-formamide / 3 h / 70 °C
2: sodium hydroxide; water / tetrahydrofuran; methanol / 1.33 h / 70 °C
3: triethylamine / N,N-dimethyl acetamide / 0.5 h / -15 - 5 °C
4: triethylamine / N,N-dimethyl acetamide / 1.5 h / -15 °C / Cooling with ice
With
water; potassium carbonate; triethylamine; sodium iodide; sodium hydroxide;
In
tetrahydrofuran; methanol; N,N-dimethyl acetamide; N,N-dimethyl-formamide;