5-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-2-furfurylchloride

Base Information

Chemical Name:5-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-2-furfurylchloride
CAS No.:118970-27-7
Molecular Formula:C₃₁H₂₅ClO₈
Molecular Weight:560.988
Hs Code.:

Synonyms:5-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-2-furfurylchloride

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Chemical Property of 5-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-2-furfurylchloride

Chemical Property:

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Technology Process of 5-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-2-furfurylchloride

There total 7 articles about 5-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-2-furfurylchloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 112969-20-7
5-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-2-furfuryl alcohol

: 118970-27-7
5-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-2-furfurylchloride

Guidance literature:: With pyridine; thionyl chloride; In benzene; at 40 ℃; for 3h;
DOI:10.1002/jhet.5570250227

Reference yield:

: 86528-49-6
2-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)furan

: 118970-27-7
5-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-2-furfurylchloride

Guidance literature:: Multi-step reaction with 5 steps

1: 39 percent / p-toluenesulfonic acid / benzene / 3 h / Heating

2: 100 percent / ammonium bromide / 0.83 h / 20 - 25 °C / electrolyzed under current of 0.01 amp at 14V

3: 86.9 percent / CF₃COOH / CH₂Cl₂ / 0.17 h / Ambient temperature

4: 88 percent / NaBH₄ / methanol; tetrahydrofuran / 0.25 h / 0 °C

5: 87 percent / SOCl₂, pyridine / benzene / 3 h / 40 °C

With pyridine; sodium tetrahydroborate; thionyl chloride; ammonium bromide; toluene-4-sulfonic acid; trifluoroacetic acid; In tetrahydrofuran; methanol; dichloromethane; benzene;
DOI:10.1002/jhet.5570250227

Reference yield:

: 108007-57-4
5-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-2-furancarboxaldehyde

: 118970-27-7
5-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-2-furfurylchloride

Guidance literature:: Multi-step reaction with 2 steps

1: 88 percent / NaBH₄ / methanol; tetrahydrofuran / 0.25 h / 0 °C

2: 87 percent / SOCl₂, pyridine / benzene / 3 h / 40 °C

With pyridine; sodium tetrahydroborate; thionyl chloride; In tetrahydrofuran; methanol; benzene;
DOI:10.1002/jhet.5570250227