Technology Process of C28H31NO4
There total 1 articles about C28H31NO4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
4-tert-butyl 1-methyl L-aspartate hydrochloride;
With
potassium carbonate;
In
tert-butyl methyl ether;
trityl chloride;
With
triethylamine;
In
acetonitrile;
for 16h;
- Guidance literature:
-
C28H31NO4;
With
potassium hexamethylsilazane;
In
tetrahydrofuran;
at -78 ℃;
for 1h;
With
oxodiperoxy(pyridine)(1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone)molybdenum (IV);
In
tetrahydrofuran;
at -78 - -55 ℃;
for 2h;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: potassium hexamethylsilazane / tetrahydrofuran / 1 h / -78 °C
1.2: 2 h / -78 - -55 °C
2.1: trifluoroacetic acid / dichloromethane / 1 h
3.1: 1,4-dioxane / 16 h
4.1: silver(l) oxide / tetrahydrofuran / 52 h / 0 - 20 °C
With
potassium hexamethylsilazane; trifluoroacetic acid; silver(l) oxide;
In
tetrahydrofuran; 1,4-dioxane; dichloromethane;