Technology Process of C26H36O5Si
There total 9 articles about C26H36O5Si which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
manganese(IV) oxide;
In
dichloromethane;
at 20 ℃;
for 6h;
DOI:10.1021/ol8008057
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: (-)-B-methoxydiisopinocamphenylborane / diethyl ether / 1 h / 0 - 20 °C
1.2: 3 h / -78 °C
2.1: sodium hydride / tetrahydrofuran / 1 h / -10 - 20 °C
2.2: 12 h / 20 °C
3.1: 9-bora-bicyclo[3.3.1]nonane / tetrahydrofuran / 5 h / 0 - 20 °C
3.2: 2 h / Reflux
4.1: dimethyl sulfoxide; triethylamine; sulfur trioxide pyridine complex / dichloromethane / 2 h / -10 °C
5.1: diethyl ether / 3 h / -78 °C
6.1: acetic acid / water / 1.5 h / 70 °C
7.1: manganese(IV) oxide / dichloromethane / 6 h / 20 °C / Sonication
With
manganese(IV) oxide; (-)-B-methoxydiisopinocamphenylborane; sulfur trioxide pyridine complex; sodium hydride; acetic acid; dimethyl sulfoxide; triethylamine; 9-bora-bicyclo[3.3.1]nonane;
In
tetrahydrofuran; diethyl ether; dichloromethane; water;
DOI:10.3987/COM-12-S(N)54
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: 9-bora-bicyclo[3.3.1]nonane / tetrahydrofuran / 5 h / 0 - 20 °C
1.2: 2 h / Reflux
2.1: dimethyl sulfoxide; triethylamine; sulfur trioxide pyridine complex / dichloromethane / 2 h / -10 °C
3.1: diethyl ether / 3 h / -78 °C
4.1: acetic acid / water / 1.5 h / 70 °C
5.1: manganese(IV) oxide / dichloromethane / 6 h / 20 °C / Sonication
With
manganese(IV) oxide; sulfur trioxide pyridine complex; acetic acid; dimethyl sulfoxide; triethylamine; 9-bora-bicyclo[3.3.1]nonane;
In
tetrahydrofuran; diethyl ether; dichloromethane; water;
DOI:10.3987/COM-12-S(N)54