Technology Process of C27H41IN2O7
There total 10 articles about C27H41IN2O7 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
osmium(VIII) oxide; 4-methylmorpholine N-oxide;
In
tetrahydrofuran; water; tert-butyl alcohol;
for 3h;
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: benzene / 3 h / Heating / reflux
2.1: titanium(IV) isopropylate / toluene / 0.17 h / 120 °C / Microwave irradiation
2.2: 2 h
3.1: trifluoroacetic acid / dichloromethane / 1.5 h / 0 °C
4.1: trimethylaluminum / dichloromethane; toluene / 0.21 h
4.2: 24 h
4.3: 2 h
5.1: potassium carbonate / N,N-dimethyl-formamide / 2.5 h
6.1: pyridine hydrogenfluoride / tetrahydrofuran; pyridine / 1 h / 0 - 20 °C
7.1: osmium(VIII) oxide; 4-methylmorpholine N-oxide / tetrahydrofuran; water; tert-butyl alcohol / 3 h
With
titanium(IV) isopropylate; osmium(VIII) oxide; trimethylaluminum; potassium carbonate; pyridine hydrogenfluoride; 4-methylmorpholine N-oxide; trifluoroacetic acid;
In
tetrahydrofuran; pyridine; dichloromethane; water; N,N-dimethyl-formamide; toluene; tert-butyl alcohol; benzene;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: titanium(IV) isopropylate / toluene / 0.17 h / 120 °C / Microwave irradiation
1.2: 2 h
2.1: trifluoroacetic acid / dichloromethane / 1.5 h / 0 °C
3.1: trimethylaluminum / dichloromethane; toluene / 0.21 h
3.2: 24 h
3.3: 2 h
4.1: potassium carbonate / N,N-dimethyl-formamide / 2.5 h
5.1: pyridine hydrogenfluoride / tetrahydrofuran; pyridine / 1 h / 0 - 20 °C
6.1: osmium(VIII) oxide; 4-methylmorpholine N-oxide / tetrahydrofuran; water; tert-butyl alcohol / 3 h
With
titanium(IV) isopropylate; osmium(VIII) oxide; trimethylaluminum; potassium carbonate; pyridine hydrogenfluoride; 4-methylmorpholine N-oxide; trifluoroacetic acid;
In
tetrahydrofuran; pyridine; dichloromethane; water; N,N-dimethyl-formamide; toluene; tert-butyl alcohol;