C₅₁H₆₂O₁₆

Base Information

Chemical Name:C₅₁H₆₂O₁₆
CAS No.:264132-58-3
Molecular Formula:C₅₁H₆₂O₁₆
Molecular Weight:931.044
Hs Code.:

C<sub>51</sub>H<sub>62</sub>O<sub>16</sub>

Synonyms:C₅₁H₆₂O₁₆

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Chemical Property of C₅₁H₆₂O₁₆

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Technology Process of C₅₁H₆₂O₁₆

There total 13 articles about C₅₁H₆₂O₁₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 264132-55-0
C₅₃H₆₃Cl₃O₁₆

: 264132-58-3
C₅₁H₆₂O₁₆

Guidance literature:: With phosphate buffer; zinc; In tetrahydrofuran; water; for 4h;
DOI:10.1021/jo991681n

Reference yield:

: ((1S,2S)-2-Benzyloxymethoxy-1-formyl-propoxy)-acetic acid tert-butyl ester

: 264132-58-3
C₅₁H₆₂O₁₆

Guidance literature:: Multi-step reaction with 12 steps

1.1: 69 percent / CuI; n-Bu₃P; PhLi / tetrahydrofuran; diethyl ether / -78 °C

2.1: trifluoroacetic acid / benzene / 0.5 h / Heating

3.1: LiHMDS; Me₃SiCl; Et₃N / hexane; tetrahydrofuran / 2 h / -78 °C

3.2: HCl / H₂O / pH 2

4.1: 95 percent / DMAP; DIC; TFA / CH₂Cl₂ / 40 °C

5.1: 82 percent / BF₃-Et₂O; Me₂S / CH₂Cl₂ / 0.17 h / 0 °C

6.1: 96 percent / imidazole / dimethylformamide / 8 h / 20 °C

7.1: 100 percent / lithium hydroxide / 2-methyl-propan-2-ol; H₂O / 2 h

8.1: 2,4,6-trichlorobenzoyl chloride; Et₃N / tetrahydrofuran / 3 h

8.2: 89 percent / DMAP / benzene / 2 h

9.1: 95 percent / HF / H₂O; acetonitrile / 0.5 h / 0 °C

10.1: 2,4,6-trichlorobenzoyl chloride; Et₃N / tetrahydrofuran / 3 h

10.2: 92 percent / DMAP; Et₃N / benzene / 2 h

11.1: 95 percent / HF / H₂O; acetonitrile / 0.5 h / 0 °C

12.1: 95 percent / phosphate buffer; zinc dust / H₂O; tetrahydrofuran / 4 h

With 1H-imidazole; dmap; lithium hydroxide; copper(l) iodide; chloro-trimethyl-silane; phosphate buffer; dimethylsulfide; tributylphosphine; 2,4,6-trichlorobenzoyl chloride; boron trifluoride diethyl etherate; hydrogen fluoride; phenyllithium; dacarbazine; triethylamine; trifluoroacetic acid; lithium hexamethyldisilazane; zinc; In tetrahydrofuran; diethyl ether; hexane; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile; tert-butyl alcohol; benzene; 1.1: Addition / 2.1: Cyclization / 3.1: Rearrangement / 3.2: Hydrolysis / 4.1: Esterification / 5.1: Hydrolysis / 6.1: Etherification / 7.1: Hydrolysis / 8.1: Substitution / 8.2: Substitution / 9.1: Hydrolysis / 10.1: Substitution / 10.2: Substitution / 11.1: Hydrolysis / 12.1: Reduction;
DOI:10.1021/jo991681n

Reference yield:

: 264132-33-4
(2S,3S,6R)-6-[(1S)-1-hydroxyethyl]-3-p-methoxybenzyloxymethyl-3,6-dihydro-2H-pyran-2-carboxylic acid 2,2,2-trichloroethyl ester

: 264132-58-3
C₅₁H₆₂O₁₆

Guidance literature:: Multi-step reaction with 7 steps

1.1: 96 percent / imidazole / dimethylformamide / 8 h / 20 °C

2.1: 100 percent / lithium hydroxide / 2-methyl-propan-2-ol; H₂O / 2 h

3.1: 2,4,6-trichlorobenzoyl chloride; Et₃N / tetrahydrofuran / 3 h

3.2: 89 percent / DMAP / benzene / 2 h

4.1: 95 percent / HF / H₂O; acetonitrile / 0.5 h / 0 °C

5.1: 2,4,6-trichlorobenzoyl chloride; Et₃N / tetrahydrofuran / 3 h

5.2: 92 percent / DMAP; Et₃N / benzene / 2 h

6.1: 95 percent / HF / H₂O; acetonitrile / 0.5 h / 0 °C

7.1: 95 percent / phosphate buffer; zinc dust / H₂O; tetrahydrofuran / 4 h

With 1H-imidazole; lithium hydroxide; phosphate buffer; 2,4,6-trichlorobenzoyl chloride; hydrogen fluoride; triethylamine; zinc; In tetrahydrofuran; water; N,N-dimethyl-formamide; acetonitrile; tert-butyl alcohol; 1.1: Etherification / 2.1: Hydrolysis / 3.1: Substitution / 3.2: Substitution / 4.1: Hydrolysis / 5.1: Substitution / 5.2: Substitution / 6.1: Hydrolysis / 7.1: Reduction;
DOI:10.1021/jo991681n