C₁₉H₁₅F₅O₇

Base Information

Chemical Name:C₁₉H₁₅F₅O₇
CAS No.:1380234-56-9
Molecular Formula:C₁₉H₁₅F₅O₇
Molecular Weight:450.316
Hs Code.:

C<sub>19</sub>H<sub>15</sub>F<sub>5</sub>O<sub>7</sub>

Synonyms:C₁₉H₁₅F₅O₇

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Chemical Property of C₁₉H₁₅F₅O₇

Chemical Property:

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Technology Process of C₁₉H₁₅F₅O₇

There total 23 articles about C₁₉H₁₅F₅O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 771-61-9
2,3,4,5,6-pentafluorophenol

: 1380234-66-1
C₁₃H₁₆O₇

: 1380234-56-9
C₁₉H₁₅F₅O₇

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 20 ℃; for 3.5h; Inert atmosphere;
DOI:10.1021/ol301090v

Reference yield:

: 1380234-61-6
C₂₃H₃₆O₆SSi

: 1380234-56-9
C₁₉H₁₅F₅O₇

Guidance literature:: Multi-step reaction with 17 steps

1.1: 2,6-dimethylpyridine / dichloromethane / 0 - 20 °C / Inert atmosphere

2.1: potassium osmate monohydrate; 4-methylmorpholine N-oxide / water; acetone / 4 h / 20 °C

3.1: 2,6-dimethylpyridine / dichloromethane / 0.42 h / -30 °C / Inert atmosphere

4.1: dmap; magnesium bromide diethyl etherate; N-ethyl-N,N-diisopropylamine / dichloromethane / 144 h / 20 °C / Inert atmosphere

5.1: potassium osmate monohydrate; 4-methylmorpholine N-oxide / water; acetone / 1 h / 20 °C

6.1: pyridinium p-toluenesulfonate / methanol / 3.5 h / 0 °C / Inert atmosphere

7.1: triethylamine / dichloromethane / 1.5 h / 0 - 20 °C / Inert atmosphere

8.1: 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride / toluene / 1.5 h / 110 °C

9.1: triethylamine; hydrazine / tetrahydrofuran; ethanol / 4.5 h / 80 °C

10.1: iodine; triethylamine / tetrahydrofuran; ethanol / 2 h / 20 °C / Inert atmosphere

11.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; tri-n-butyl-tin hydride / benzene / 1.5 h / 20 °C / Inert atmosphere

12.1: pyridinium p-toluenesulfonate / ethanol / 120 h / 20 °C / Inert atmosphere

13.1: sodium hypochlorite; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; tetra-(n-butyl)ammonium iodide; sodium hydrogencarbonate; potassium bromide / dichloromethane; water / 2.5 h / 0 - 20 °C

13.2: 1.5 h / 20 °C

14.1: potassium carbonate / N,N-dimethyl-formamide / 1.5 h / 20 °C

15.1: potassium hexamethylsilazane / tetrahydrofuran; toluene / 0.08 h / -78 °C / Inert atmosphere

16.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; phenylsilane / dichloromethane / 4 h / 20 °C / Inert atmosphere

17.1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 3.5 h / 20 °C / Inert atmosphere

With 2,6-dimethylpyridine; dmap; sodium hypochlorite; tetrakis(triphenylphosphine) palladium⁽⁰⁾; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; magnesium bromide diethyl etherate; 2,2'-azobis(isobutyronitrile); potassium osmate monohydrate; phenylsilane; iodine; tri-n-butyl-tin hydride; pyridinium p-toluenesulfonate; tetra-(n-butyl)ammonium iodide; potassium hexamethylsilazane; sodium hydrogencarbonate; potassium carbonate; 4-methylmorpholine N-oxide; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N-ethyl-N,N-diisopropylamine; potassium bromide; hydrazine; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; N,N-dimethyl-formamide; acetone; toluene; benzene; 6.1: Barton-McCombie deoxygenation / 11.1: Stille coupling;
DOI:10.1021/ol301090v

Reference yield:

: 1380234-65-0
C₂₂H₃₆O₈Si

: 1380234-56-9
C₁₉H₁₅F₅O₇

Guidance literature:: Multi-step reaction with 3 steps

1: potassium hexamethylsilazane / tetrahydrofuran; toluene / 0.08 h / -78 °C / Inert atmosphere

2: tetrakis(triphenylphosphine) palladium⁽⁰⁾; phenylsilane / dichloromethane / 4 h / 20 °C / Inert atmosphere

3: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 3.5 h / 20 °C / Inert atmosphere

With dmap; tetrakis(triphenylphosphine) palladium⁽⁰⁾; phenylsilane; potassium hexamethylsilazane; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In tetrahydrofuran; dichloromethane; toluene;
DOI:10.1021/ol301090v