N-[3-(3,4-dimethylphenylamino)pyridin-4-yl]trifluoromethanesulfonamide

Base Information

Chemical Name:N-[3-(3,4-dimethylphenylamino)pyridin-4-yl]trifluoromethanesulfonamide
CAS No.:1580456-09-2
Molecular Formula:C₁₄H₁₄F₃N₃O₂S
Molecular Weight:345.345
Hs Code.:

Synonyms:N-[3-(3,4-dimethylphenylamino)pyridin-4-yl]trifluoromethanesulfonamide

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Chemical Property of N-[3-(3,4-dimethylphenylamino)pyridin-4-yl]trifluoromethanesulfonamide

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Technology Process of N-[3-(3,4-dimethylphenylamino)pyridin-4-yl]trifluoromethanesulfonamide

There total 5 articles about N-[3-(3,4-dimethylphenylamino)pyridin-4-yl]trifluoromethanesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

: 421-83-0
trifluoromethane sulfonyl chloride

: 1580456-02-5
4-amino-3-(3,4-dimethylphenylamino)pyridine

: 1580456-09-2
N-[3-(3,4-dimethylphenylamino)pyridin-4-yl]trifluoromethanesulfonamide

Guidance literature:: 4-amino-3-(3,4-dimethylphenylamino)pyridine; With potassium carbonate; In acetonitrile; for 0.0833333h;

trifluoromethane sulfonyl chloride; In acetonitrile;
DOI:10.1016/j.ejmech.2013.12.033

Reference yield:

: 626-55-1,163928-56-1
3-Bromopyridine

: 1580456-09-2
N-[3-(3,4-dimethylphenylamino)pyridin-4-yl]trifluoromethanesulfonamide

Guidance literature:: Multi-step reaction with 5 steps

1: dihydrogen peroxide / acetic acid

2: nitric acid; sulfuric acid

3: pyridine / 70 °C

4: iron; water / acetic acid / Reflux

5: potassium carbonate / acetonitrile / 0.08 h

With pyridine; sulfuric acid; water; dihydrogen peroxide; nitric acid; iron; potassium carbonate; In acetic acid; acetonitrile;
DOI:10.1016/j.ejmech.2013.12.033

Reference yield:

: 2402-97-3
3-bromopyridine N-oxide

: 1580456-09-2
N-[3-(3,4-dimethylphenylamino)pyridin-4-yl]trifluoromethanesulfonamide

Guidance literature:: Multi-step reaction with 4 steps

1: nitric acid; sulfuric acid

2: pyridine / 70 °C

3: iron; water / acetic acid / Reflux

4: potassium carbonate / acetonitrile / 0.08 h

With pyridine; sulfuric acid; water; nitric acid; iron; potassium carbonate; In acetic acid; acetonitrile;
DOI:10.1016/j.ejmech.2013.12.033