Beryllium;benzo[h]quinolin-10-olate

Base Information

• Chemical Name: Beryllium;benzo[h]quinolin-10-olate
• CAS No.: 148896-39-3
• Molecular Formula: C26H16BeN2O2
• Molecular Weight: 397.437
• European Community (EC) Number: 890-452-2
• Mol file: 148896-39-3.mol

Synonyms:148896-39-3;Bepq2;beryllium;benzo[h]quinolin-10-olate;BeBq2;Bis(10-hydroxybenzo[h]-quinolinato)beryllium

Chemical Property of Beryllium;benzo[h]quinolin-10-olate

Chemical Property:

• PSA: 44.24000
• LogP: 6.46220
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 2
• Exact Mass: 397.1333608
• Heavy Atom Count: 31
• Complexity: 516

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: [Be+2].C1=CC2=C(C(=C1)[O-])C3=C(C=CC=N3)C=C2.C1=CC2=C(C(=C1)[O-])C3=C(C=CC=N3)C=C2
• Description: Bis(10-hydroxybenzo[h]quinolinato)beryllium, known as Bebq2, is the brother of Bepp2 in?the?Beryllium complex family. It is also a blue-fluorescence?emitter with excellent charge transport ability.

Technology Process of Beryllium;benzo[h]quinolin-10-olate

There total 2 articles about Beryllium;benzo[h]quinolin-10-olate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

beryllium(II) sulphate tetrahydrate + benzo[h]quinolin-10-ol (33155-90-7) → bis(10-hydroxybenzo[h]quinolinato) beryllium (148896-39-3)

Guidance literature:

With sodium hydroxide; In ethanol; water; ligand dissolved in EtOH; metal salt dissolved in H2O in another flask; soln. of ligand was slowly poured into soln. of metal salt with stirring; complex deposited after the mixed soln. was adjusted to pH 10 using NaOH; filtered; washed (EtOH);

DOI:10.1016/j.saa.2006.11.042

Reference yield:

→ bis(10-hydroxybenzo[h]quinolinato) beryllium (148896-39-3)

Guidance literature:

With sodium hydroxide; In methanol;

upstream raw materials:

benzo[h]quinolin-10-ol

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