(2E,N′E)-N′-(3-((bis(2-hydroxyethyl)amino)methyl)-2-hydroxy-5-methylbenzylidene)-2-(hydroxyimino)propanehydrazide

Base Information

Chemical Name:(2E,N′E)-N′-(3-((bis(2-hydroxyethyl)amino)methyl)-2-hydroxy-5-methylbenzylidene)-2-(hydroxyimino)propanehydrazide
CAS No.:1428521-92-9
Molecular Formula:C₁₆H₂₄N₄O₅
Molecular Weight:352.39
Hs Code.:

Synonyms:(2E,N′E)-N′-(3-((bis(2-hydroxyethyl)amino)methyl)-2-hydroxy-5-methylbenzylidene)-2-(hydroxyimino)propanehydrazide

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Chemical Property of (2E,N′E)-N′-(3-((bis(2-hydroxyethyl)amino)methyl)-2-hydroxy-5-methylbenzylidene)-2-(hydroxyimino)propanehydrazide

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Technology Process of (2E,N′E)-N′-(3-((bis(2-hydroxyethyl)amino)methyl)-2-hydroxy-5-methylbenzylidene)-2-(hydroxyimino)propanehydrazide

There total 2 articles about (2E,N′E)-N′-(3-((bis(2-hydroxyethyl)amino)methyl)-2-hydroxy-5-methylbenzylidene)-2-(hydroxyimino)propanehydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.8%

: 1428521-93-0
3-((bis(2-hydroxyethyl)-amino)methyl)-2-hydroxy-5-methylbenzaldehyde

: (E)-2-(hydroxyimino)propanehydrazide

: 1428521-92-9
(2E,N′E)-N′-(3-((bis(2-hydroxyethyl)amino)methyl)-2-hydroxy-5-methylbenzylidene)-2-(hydroxyimino)propanehydrazide

Guidance literature:: In methanol; at 60 ℃; for 12h; Inert atmosphere;
DOI:10.1021/ic400091j

Reference yield:

: 613-84-3
2-hydroxy-5-methylbenzaldehyde

: 1428521-92-9
(2E,N′E)-N′-(3-((bis(2-hydroxyethyl)amino)methyl)-2-hydroxy-5-methylbenzylidene)-2-(hydroxyimino)propanehydrazide

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogenchloride; sulfuric acid / water / 6 h / 75 °C

2: triethylamine / tetrahydrofuran / 24 h / 20 °C / Inert atmosphere

3: methanol / 12 h / 60 °C / Inert atmosphere

With hydrogenchloride; sulfuric acid; triethylamine; In tetrahydrofuran; methanol; water;
DOI:10.1021/ic400091j