1-{4-[4-(dimethylamino)phenyl]buta-1,3-diynyl}-9-methyl-1,9-dihydro(C₆₀-Ih)[5,6]fullerene

Base Information

• Chemical Name: 1-{4-[4-(dimethylamino)phenyl]buta-1,3-diynyl}-9-methyl-1,9-dihydro(C₆₀-Ih)[5,6]fullerene
• CAS No.: 1231756-16-3
• Molecular Formula: C₇₃H₁₃N
• Molecular Weight: 903.913

Synonyms:1-{4-[4-(dimethylamino)phenyl]buta-1,3-diynyl}-9-methyl-1,9-dihydro(C₆₀-Ih)[5,6]fullerene

Chemical Property of 1-{4-[4-(dimethylamino)phenyl]buta-1,3-diynyl}-9-methyl-1,9-dihydro(C₆₀-Ih)[5,6]fullerene

Chemical Property:

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Technology Process of 1-{4-[4-(dimethylamino)phenyl]buta-1,3-diynyl}-9-methyl-1,9-dihydro(C₆₀-Ih)[5,6]fullerene

There total 1 articles about 1-{4-[4-(dimethylamino)phenyl]buta-1,3-diynyl}-9-methyl-1,9-dihydro(C₆₀-Ih)[5,6]fullerene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

4-ethynyl-N,N-dimethylaniline (17573-94-3,752235-18-0) + 1-ethynyl-9-methyl-1,9-dihydro(C60-Ih)[5,6]fullerene (182758-93-6) → 1-{4-[4-(dimethylamino)phenyl]buta-1,3-diynyl}-9-methyl-1,9-dihydro(C60-Ih)[5,6]fullerene (1231756-16-3)

Guidance literature:

With N,N,N,N,-tetramethylethylenediamine; copper(l) chloride; In chlorobenzene; at 20 ℃; for 4h;

DOI:10.1002/anie.200906853

Reference yield: 97.0%

1-{4-[4-(dimethylamino)phenyl]buta-1,3-diynyl}-9-methyl-1,9-dihydro(C60-Ih)[5,6]fullerene (1231756-16-3) + ethenetetracarbonitrile (670-54-2) → C79H13N5 (1231756-06-1)

Guidance literature:

In chlorobenzene; at 20 ℃; for 12h; Inert atmosphere;

DOI:10.1002/anie.200906853

upstream raw materials:

4-ethynyl-N,N-dimethylaniline

1-ethynyl-9-methyl-1,9-dihydro(C₆₀-Ih)[5,6]fullerene

Downstream raw materials:

C₇₉H₁₃N₅

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