C₄₂⁽¹³⁾CH₃₈O₆

Base Information

Chemical Name:C₄₂⁽¹³⁾CH₃₈O₆
CAS No.:357409-20-2
Molecular Formula:C₄₃H₃₈O₆
Molecular Weight:651.76
Hs Code.:

C<sub>42</sub><sup>(13)</sup>CH<sub>38</sub>O<sub>6</sub>

Synonyms:C₄₂⁽¹³⁾CH₃₈O₆

Suppliers and Price of C₄₂⁽¹³⁾CH₃₈O₆

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₄₂⁽¹³⁾CH₃₈O₆

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₄₂⁽¹³⁾CH₃₈O₆

There total 9 articles about C₄₂⁽¹³⁾CH₃₈O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 357409-16-6
C₆₁⁽¹³⁾CH₅₂O₁₃

: 357409-20-2
C₄₂⁽¹³⁾CH₃₈O₆

Guidance literature:: With potassium hydroxide; In methanol; water;
DOI:10.1002/1099-0690(200106)2001:12<2379::AID-EJOC2379>3.0.CO;2-D

Reference yield:

: 5447-02-9
3,4-dibenzyloxybenzaldehyde

: 357409-20-2
C₄₂⁽¹³⁾CH₃₈O₆

Guidance literature:: Multi-step reaction with 6 steps

1.1: 86 percent / NaH / dimethylformamide / 2 h / 20 °C

2.1: NaBH₄ / 1,2-dimethoxy-ethane / 0.08 h / 85 °C

2.2: BF₃*Et₂O / ethyl acetate; CH₂Cl₂ / 0.33 h / 20 °C

3.1: NMO / OsO₄ / tetrahydrofuran; H₂O; 2-methyl-propan-2-ol / 6 h / 20 °C

4.1: 80 percent / NaBH₃CN / acetic acid / 48 h

5.1: DCC / 4-DMAP / CH₂Cl₂ / 2.5 h / Heating

6.1: 97 percent / KOH / methanol; H₂O

With potassium hydroxide; sodium tetrahydroborate; N-methyl-2-indolinone; sodium hydride; sodium cyanoborohydride; dicyclohexyl-carbodiimide; dmap; osmium(VIII) oxide; In tetrahydrofuran; methanol; 1,2-dimethoxyethane; dichloromethane; water; acetic acid; N,N-dimethyl-formamide; tert-butyl alcohol;
DOI:10.1002/1099-0690(200106)2001:12<2379::AID-EJOC2379>3.0.CO;2-D

Reference yield:

: 59434-20-7
1,3,5-tri-O-benzylphloroglucinol

: 357409-20-2
C₄₂⁽¹³⁾CH₃₈O₆

Guidance literature:: Multi-step reaction with 8 steps

1.1: 64 percent / TFAA / CH₂Cl₂ / 1.5 h / 0 °C

2.1: 80 percent / TiCl₄ / CH₂Cl₂ / 2.67 h / 0 °C

3.1: 86 percent / NaH / dimethylformamide / 2 h / 20 °C

4.1: NaBH₄ / 1,2-dimethoxy-ethane / 0.08 h / 85 °C

4.2: BF₃*Et₂O / ethyl acetate; CH₂Cl₂ / 0.33 h / 20 °C

5.1: NMO / OsO₄ / tetrahydrofuran; H₂O; 2-methyl-propan-2-ol / 6 h / 20 °C

6.1: 80 percent / NaBH₃CN / acetic acid / 48 h

7.1: DCC / 4-DMAP / CH₂Cl₂ / 2.5 h / Heating

8.1: 97 percent / KOH / methanol; H₂O

With potassium hydroxide; sodium tetrahydroborate; N-methyl-2-indolinone; titanium tetrachloride; sodium hydride; sodium cyanoborohydride; dicyclohexyl-carbodiimide; trifluoroacetic anhydride; dmap; osmium(VIII) oxide; In tetrahydrofuran; methanol; 1,2-dimethoxyethane; dichloromethane; water; acetic acid; N,N-dimethyl-formamide; tert-butyl alcohol;
DOI:10.1002/1099-0690(200106)2001:12<2379::AID-EJOC2379>3.0.CO;2-D