glutaric acid (4,5-dimethoxy-2-nitrobenzyl) ester (4-chloro-2-nitrobenzyl) ester

Base Information

Chemical Name:glutaric acid (4,5-dimethoxy-2-nitrobenzyl) ester (4-chloro-2-nitrobenzyl) ester
CAS No.:724763-05-7
Molecular Formula:C₂₁H₂₁ClN₂O₁₀
Molecular Weight:496.858
Hs Code.:

Synonyms:glutaric acid (4,5-dimethoxy-2-nitrobenzyl) ester (4-chloro-2-nitrobenzyl) ester

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Chemical Property of glutaric acid (4,5-dimethoxy-2-nitrobenzyl) ester (4-chloro-2-nitrobenzyl) ester

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Technology Process of glutaric acid (4,5-dimethoxy-2-nitrobenzyl) ester (4-chloro-2-nitrobenzyl) ester

There total 7 articles about glutaric acid (4,5-dimethoxy-2-nitrobenzyl) ester (4-chloro-2-nitrobenzyl) ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 22996-18-5
(4-chloro-2-nitrophenyl)methanol

: 457612-05-4
glutaric acid mono-(4,5-dimethoxy-2-nitrobenzyl) ester

: 724763-05-7
glutaric acid (4,5-dimethoxy-2-nitrobenzyl) ester (4-chloro-2-nitrobenzyl) ester

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In chloroform; at 60 ℃; for 24h;
DOI:10.1021/ja049686b

Reference yield:

: 108-55-4
glutaric anhydride,

: 724763-05-7
glutaric acid (4,5-dimethoxy-2-nitrobenzyl) ester (4-chloro-2-nitrobenzyl) ester

Guidance literature:: Multi-step reaction with 2 steps

1: 56 percent / 4-dimethylaminopyridine; pyridine / 24 h / 50 °C

2: 76 percent / 4-dimethylaminopyridine; N,N'-dicyclohexylcarbodiimide / CHCl₃ / 24 h / 60 °C

With pyridine; dmap; dicyclohexyl-carbodiimide; In chloroform;
DOI:10.1021/ja049686b

Reference yield:

: 1016-58-6
6-nitroveratryl alcohol

: 724763-05-7
glutaric acid (4,5-dimethoxy-2-nitrobenzyl) ester (4-chloro-2-nitrobenzyl) ester

Guidance literature:: Multi-step reaction with 2 steps

1: 56 percent / 4-dimethylaminopyridine; pyridine / 24 h / 50 °C

2: 76 percent / 4-dimethylaminopyridine; N,N'-dicyclohexylcarbodiimide / CHCl₃ / 24 h / 60 °C

With pyridine; dmap; dicyclohexyl-carbodiimide; In chloroform;
DOI:10.1021/ja049686b