(+)-(S)-(N-3,5-dinitrobenzoyl)-3-amino-N-10-undecenyl-ε-caprolactam

Base Information

Chemical Name:(+)-(S)-(N-3,5-dinitrobenzoyl)-3-amino-N-10-undecenyl-ε-caprolactam
CAS No.:1334523-91-9
Molecular Formula:C₂₄H₃₄N₄O₆
Molecular Weight:474.557
Hs Code.:

Synonyms:(+)-(S)-(N-3,5-dinitrobenzoyl)-3-amino-N-10-undecenyl-ε-caprolactam

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Chemical Property of (+)-(S)-(N-3,5-dinitrobenzoyl)-3-amino-N-10-undecenyl-ε-caprolactam

Chemical Property:

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Technology Process of (+)-(S)-(N-3,5-dinitrobenzoyl)-3-amino-N-10-undecenyl-ε-caprolactam

There total 6 articles about (+)-(S)-(N-3,5-dinitrobenzoyl)-3-amino-N-10-undecenyl-ε-caprolactam which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1334523-94-2
(N-3,5-dinitrobenzoyl)-3-amino-N-10-undecenyl-ε-caprolactam

: 1334523-91-9
(+)-(S)-(N-3,5-dinitrobenzoyl)-3-amino-N-10-undecenyl-ε-caprolactam

Guidance literature:: With column with (S)-N-(1-naphthyl)leucine-derived chiral stationary phase; In hexane; isopropyl alcohol; optical yield given as %ee; Resolution of racemate;
DOI:10.1016/j.tet.2011.06.103

Reference yield:

: C₂₅H₃₄N₂O₃

: 1334523-91-9
(+)-(S)-(N-3,5-dinitrobenzoyl)-3-amino-N-10-undecenyl-ε-caprolactam

Guidance literature:: Multi-step reaction with 3 steps

1: hydrazine hydrate / ethanol / 6 h / Reflux

2: triethylamine / dichloromethane / 0.5 h / 20 °C / Cooling with ice

3: column with (S)-N-(1-naphthyl)leucine-derived chiral stationary phase / hexane; isopropyl alcohol / Resolution of racemate

With hydrazine hydrate; triethylamine; In ethanol; hexane; dichloromethane; isopropyl alcohol;
DOI:10.1016/j.tet.2011.06.103

Reference yield:

: 99-33-2
3,5-dinitrobenoyl chloride

: 1334523-91-9
(+)-(S)-(N-3,5-dinitrobenzoyl)-3-amino-N-10-undecenyl-ε-caprolactam

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / 0.5 h / 20 °C / Cooling with ice

2: column with (S)-N-(1-naphthyl)leucine-derived chiral stationary phase / hexane; isopropyl alcohol / Resolution of racemate

With triethylamine; In hexane; dichloromethane; isopropyl alcohol;
DOI:10.1016/j.tet.2011.06.103