C₁₉H₃₀O₃

Base Information

Chemical Name:C₁₉H₃₀O₃
CAS No.:1310801-70-7
Molecular Formula:C₁₉H₃₀O₃
Molecular Weight:306.445
Hs Code.:

C<sub>19</sub>H<sub>30</sub>O<sub>3</sub>

Synonyms:C₁₉H₃₀O₃

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Chemical Property of C₁₉H₃₀O₃

Chemical Property:

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Technology Process of C₁₉H₃₀O₃

There total 11 articles about C₁₉H₃₀O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1310801-69-4
C₁₈H₂₈O₄

: 1310801-70-7
C₁₉H₃₀O₃

Guidance literature:: With n-butyllithium; methyl-triphenylphosphonium iodide; In tetrahydrofuran; at 0 - 20 ℃;
DOI:10.1016/j.tetlet.2011.03.089

Reference yield:

: 1310801-68-3
C₁₈H₃₀O₄

: 1310801-70-7
C₁₉H₃₀O₃

Guidance literature:: Multi-step reaction with 2 steps

1: oxalyl dichloride; dimethyl sulfoxide; triethylamine / dichloromethane / 1 h / -78 °C

2: n-butyllithium; methyl-triphenylphosphonium iodide / tetrahydrofuran / 0 - 20 °C

With n-butyllithium; oxalyl dichloride; methyl-triphenylphosphonium iodide; dimethyl sulfoxide; triethylamine; In tetrahydrofuran; dichloromethane; 1: Swern oxidation / 2: Wittig reaction;
DOI:10.1016/j.tetlet.2011.03.089

Reference yield:

: C₁₄H₂₁NO₃

: 1310801-70-7
C₁₉H₃₀O₃

Guidance literature:: Multi-step reaction with 7 steps

1: 1,8-diazabicyclo[5.4.0]undec-7-ene; lithium chloride / dimethyl sulfoxide / 0.25 h / 0 °C

2: methanol; copper diacetate; ammonium chloride / dimethyl sulfoxide / 24 h / 20 °C

3: sodium tetrahydroborate; nickel (II) chloride hexahydrate / methanol / 3 h / 0 - 20 °C

4: N-ethyl-N,N-diisopropylamine / dichloromethane / 6 h / 0 - 20 °C

5: diisobutylaluminium hydride / dichloromethane / 0.25 h / 0 °C

6: oxalyl dichloride; dimethyl sulfoxide; triethylamine / dichloromethane / 1 h / -78 °C

7: n-butyllithium; methyl-triphenylphosphonium iodide / tetrahydrofuran / 0 - 20 °C

With methanol; sodium tetrahydroborate; n-butyllithium; oxalyl dichloride; nickel (II) chloride hexahydrate; copper diacetate; methyl-triphenylphosphonium iodide; diisobutylaluminium hydride; ammonium chloride; dimethyl sulfoxide; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; N-ethyl-N,N-diisopropylamine; lithium chloride; In tetrahydrofuran; methanol; dichloromethane; dimethyl sulfoxide; 1: Horner-Wadsworth-Emmons olefination / 6: Swern oxidation / 7: Wittig reaction;
DOI:10.1016/j.tetlet.2011.03.089