4-Methyl-benzenesulfinic acid phenylselanylmethyl ester

Base Information

Chemical Name:4-Methyl-benzenesulfinic acid phenylselanylmethyl ester
CAS No.:79665-11-5
Molecular Formula:C₁₄H₁₄O₂SSe
Molecular Weight:325.29
Hs Code.:

Synonyms:4-Methyl-benzenesulfinic acid phenylselanylmethyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-Methyl-benzenesulfinic acid phenylselanylmethyl ester

Chemical Property:

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Technology Process of 4-Methyl-benzenesulfinic acid phenylselanylmethyl ester

There total 3 articles about 4-Methyl-benzenesulfinic acid phenylselanylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 186581-53-3,908094-01-9,334-88-3
diazomethane

: 68819-94-3
p-tolyl benzeneselenosulfonate

: 672-78-6
methyl p-toluene sulfinate

: 79665-11-5
4-Methyl-benzenesulfinic acid phenylselanylmethyl ester

: 79665-10-4
(phenylseleno)methyl p-tolylsulfone

: 79665-09-1
1-(phenylseleno)-2-(p-toluenesulfonyl)ethane

Guidance literature:: In diethyl ether; dichloromethane; for 0.5h; Further byproducts given; Irradiation;
DOI:10.1021/jo00339a049

Reference yield:

: 186581-53-3,908094-01-9,334-88-3
diazomethane

: 68819-94-3
p-tolyl benzeneselenosulfonate

: 1666-13-3
diphenyl diselenide

: 672-78-6
methyl p-toluene sulfinate

: 79665-11-5
4-Methyl-benzenesulfinic acid phenylselanylmethyl ester

: 79665-10-4
(phenylseleno)methyl p-tolylsulfone

Guidance literature:: In diethyl ether; dichloromethane; for 17h; Yield given. Yields of byproduct given; Ambient temperature;
DOI:10.1021/jo00339a049

Reference yield:

: 186581-53-3,908094-01-9,334-88-3
diazomethane

: 68819-94-3
p-tolyl benzeneselenosulfonate

: 1666-13-3
diphenyl diselenide

: 672-78-6
methyl p-toluene sulfinate

: 79665-11-5
4-Methyl-benzenesulfinic acid phenylselanylmethyl ester

: 79665-10-4
(phenylseleno)methyl p-tolylsulfone

: 79665-09-1
1-(phenylseleno)-2-(p-toluenesulfonyl)ethane

Guidance literature:: In diethyl ether; dichloromethane; for 0.5h; Product distribution; Irradiation; also in the dark, other time;
DOI:10.1021/jo00339a049