7-bromo-2-isoquinolin-3-ylchromen-4-one O-tert-butyl oxime

Base Information

Chemical Name:7-bromo-2-isoquinolin-3-ylchromen-4-one O-tert-butyl oxime
CAS No.:1300033-83-3
Molecular Formula:C₂₂H₁₉BrN₂O₂
Molecular Weight:423.309
Hs Code.:

Synonyms:7-bromo-2-isoquinolin-3-ylchromen-4-one O-tert-butyl oxime

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Chemical Property of 7-bromo-2-isoquinolin-3-ylchromen-4-one O-tert-butyl oxime

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Technology Process of 7-bromo-2-isoquinolin-3-ylchromen-4-one O-tert-butyl oxime

There total 1 articles about 7-bromo-2-isoquinolin-3-ylchromen-4-one O-tert-butyl oxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 30186-18-6
4'-bromo-2'-hydroxyacetophenone

: 1300033-83-3
7-bromo-2-isoquinolin-3-ylchromen-4-one O-tert-butyl oxime

Guidance literature:: Multi-step reaction with 2 steps

1.1: pyridine; sodium hydride / mineral oil / 1 h / 90 °C

1.2: 1 h / 110 °C

2.1: ethanol / 12 h / 120 °C / Sealed tube

With pyridine; sodium hydride; In ethanol; mineral oil;
DOI:10.1021/acs.jmedchem.7b00991

Reference yield: 91.0%

: 1300033-83-3
7-bromo-2-isoquinolin-3-ylchromen-4-one O-tert-butyl oxime

: 98-80-6
phenylboronic acid

: 1300034-04-1
2-isoquinolin-3-yl-7-phenyI-chromen-4-one O-tert-butyl oxime

Guidance literature:: With sodium carbonate; In ethanol; water; toluene; at 120 ℃; for 4h; Inert atmosphere; Sealed tube;

Reference yield: 76.0%

: 1300033-83-3
7-bromo-2-isoquinolin-3-ylchromen-4-one O-tert-butyl oxime

: 6783-05-7
trans-2-phenylvinylboronic acid

: 1300033-89-9
2-isoquinolin-3-yl-7-((E)styryl)-chromen-4-one O-tert-butyl oxime

Guidance literature:: With cesium fluoride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In methanol; 1,2-dimethoxyethane; at 150 ℃; for 0.0833333h; Inert atmosphere; Microwave irradiation;