1-(3,4-dimethoxy-5-nitrophenyl)-2-nitroethane

Base Information

Chemical Name:1-(3,4-dimethoxy-5-nitrophenyl)-2-nitroethane
CAS No.:114547-22-7
Molecular Formula:C₁₀H₁₂N₂O₆
Molecular Weight:256.215
Hs Code.:

Synonyms:1-(3,4-dimethoxy-5-nitrophenyl)-2-nitroethane

Suppliers and Price of 1-(3,4-dimethoxy-5-nitrophenyl)-2-nitroethane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 1-(3,4-dimethoxy-5-nitrophenyl)-2-nitroethane

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1-(3,4-dimethoxy-5-nitrophenyl)-2-nitroethane

There total 2 articles about 1-(3,4-dimethoxy-5-nitrophenyl)-2-nitroethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 22027-96-9
5-nitroveratral

: 114547-22-7
1-(3,4-dimethoxy-5-nitrophenyl)-2-nitroethane

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / NH₄OAc

2: 90 percent / NaBH₄, silica gel

With sodium tetrahydroborate; ammonium acetate; silica gel;
DOI:10.1016/S0960-894X(98)00138-3

Reference yield:

: 6635-20-7
isonitrovanillin

: 114547-22-7
1-(3,4-dimethoxy-5-nitrophenyl)-2-nitroethane

Guidance literature:: Multi-step reaction with 3 steps

1: 81 percent / sodium hydroxyde, benzyltributylammonium bromide / CH₂Cl₂ / 24 h

2: 78 percent / ammonium acetate / acetic acid / 3 h / 100 °C

3: 92 percent / sodium borohydride / methanol; ethyl acetate / 0.25 h / 0 °C

With ammonium acetate; sodium hydroxide; sodium tetrahydroborate; benzyl tri-n-butylammonium bromide; In methanol; dichloromethane; acetic acid; ethyl acetate;
DOI:10.1016/S0040-4020(01)87665-1

Reference yield: 95.0%

: 114547-22-7
1-(3,4-dimethoxy-5-nitrophenyl)-2-nitroethane

: 114547-23-8
2,3-dimethoxy-5-(2-nitroethyl)aniline

Guidance literature:: With hydrogen; platinum(IV) oxide; In acetic acid; for 3h; under 760 Torr; Ambient temperature;
DOI:10.1016/S0040-4020(01)87665-1