(S)-3-<(tert-butoxycarbonyl)amino>-N-cyclohexyl-N-<(ethoxycarbonyl)methyl>succinamic acid tert-butyl ester

Base Information

• Chemical Name: (S)-3-<(tert-butoxycarbonyl)amino>-N-cyclohexyl-N-<(ethoxycarbonyl)methyl>succinamic acid tert-butyl ester
• CAS No.: 155541-30-3
• Molecular Formula: C₂₃H₄₀N₂O₇
• Molecular Weight: 456.58

Synonyms:(S)-3-<(tert-butoxycarbonyl)amino>-N-cyclohexyl-N-<(ethoxycarbonyl)methyl>succinamic acid tert-butyl ester

Chemical Property of (S)-3-<(tert-butoxycarbonyl)amino>-N-cyclohexyl-N-<(ethoxycarbonyl)methyl>succinamic acid tert-butyl ester

Chemical Property:

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Technology Process of (S)-3-<(tert-butoxycarbonyl)amino>-N-cyclohexyl-N-<(ethoxycarbonyl)methyl>succinamic acid tert-butyl ester

There total 2 articles about (S)-3-<(tert-butoxycarbonyl)amino>-N-cyclohexyl-N-<(ethoxycarbonyl)methyl>succinamic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

ethyl N-cyclohexylglycinate (37883-45-7) + Boc-Asp(OtBu)-OH (1676-90-0) → (S)-3-<(tert-butoxycarbonyl)amino>-N-cyclohexyl-N-<(ethoxycarbonyl)methyl>succinamic acid tert-butyl ester (155541-30-3)

Guidance literature:

With N-ethylmorpholine;; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; In N,N-dimethyl-formamide;

DOI:10.1021/jm00049a008

Reference yield:

N-ethylmorpholine; (100-74-3) + ethyl N-cyclohexylglycinate (37883-45-7) + Boc-Asp(OtBu)-OH (1676-90-0) + (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate (56602-33-6) → (S)-3-<(tert-butoxycarbonyl)amino>-N-cyclohexyl-N-<(ethoxycarbonyl)methyl>succinamic acid tert-butyl ester (155541-30-3)

Guidance literature:

In N,N-dimethyl-formamide;

Reference yield:

(S)-3-<(tert-butoxycarbonyl)amino>-N-cyclohexyl-N-<(ethoxycarbonyl)methyl>succinamic acid tert-butyl ester (155541-30-3) → (S)-3-Amino-N-cyclohexyl-N-ethoxycarbonylmethyl-succinamic acid tert-butyl ester (1026676-23-2)

Guidance literature:

With toluene-4-sulfonic acid; In acetonitrile; for 8h; Ambient temperature;

DOI:10.1021/jm00049a008

upstream raw materials:

ethyl N-cyclohexylglycinate

Boc-Asp(OtBu)-OH

N-ethylmorpholine;

(benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate

Downstream raw materials:

(S)-3-Amino-N-cyclohexyl-N-ethoxycarbonylmethyl-succinamic acid tert-butyl ester

(S)-N-Cyclohexyl-N-ethoxycarbonylmethyl-3-(naphthalene-2-sulfonylamino)-succinamic acid

(S)-N-cyclohexyl-N-<(ethoxycarbonyl)methyl>-3-<(naphth-2-ylsulfonyl)amino>succinamic acid tert-butyl ester

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