O-{3-[bis(p-toluenesulfonyl)amino]-1-methylbutyl} O-(p-tolyl)thiocarbonate

Base Information

Chemical Name:O-{3-[bis(p-toluenesulfonyl)amino]-1-methylbutyl} O-(p-tolyl)thiocarbonate
CAS No.:497069-45-1
Molecular Formula:C₂₇H₃₁NO₆S₃
Molecular Weight:561.744
Hs Code.:

Synonyms:O-{3-[bis(p-toluenesulfonyl)amino]-1-methylbutyl} O-(p-tolyl)thiocarbonate

Suppliers and Price of O-{3-[bis(p-toluenesulfonyl)amino]-1-methylbutyl} O-(p-tolyl)thiocarbonate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of O-{3-[bis(p-toluenesulfonyl)amino]-1-methylbutyl} O-(p-tolyl)thiocarbonate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of O-{3-[bis(p-toluenesulfonyl)amino]-1-methylbutyl} O-(p-tolyl)thiocarbonate

There total 6 articles about O-{3-[bis(p-toluenesulfonyl)amino]-1-methylbutyl} O-(p-tolyl)thiocarbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 937-63-3
p-Tolyl chlorothionoformate

: 497069-47-3
C₁₉H₂₅NO₅S₂

: 497069-45-1
O-{3-[bis(p-toluenesulfonyl)amino]-1-methylbutyl} O-(p-tolyl)thiocarbonate

Guidance literature:: With pyridine; In dichloromethane; at 20 ℃; for 16h;
DOI:10.1002/1099-0690(200208)2002:16<2742::AID-EJOC2742>3.0.CO;2-R

Reference yield:

: 2-(tert-butyldimethylsilanyloxy)-4-[bis(p-toluenesulfonyl)amino]pentane

: 497069-45-1
O-{3-[bis(p-toluenesulfonyl)amino]-1-methylbutyl} O-(p-tolyl)thiocarbonate

Guidance literature:: Multi-step reaction with 2 steps

1: HF*pyridine / CH₂Cl₂ / 0 - 20 °C

2: 95 percent / pyridine / CH₂Cl₂ / 16 h / 20 °C

With pyridine; pyridine hydrogenfluoride; In dichloromethane;
DOI:10.1002/1099-0690(200208)2002:16<2742::AID-EJOC2742>3.0.CO;2-R

Reference yield:

: N-(3-hydroxy-1-methylbutyl)-p-toluenesulfonamide

: 497069-45-1
O-{3-[bis(p-toluenesulfonyl)amino]-1-methylbutyl} O-(p-tolyl)thiocarbonate

Guidance literature:: Multi-step reaction with 4 steps

1.1: dimethylformamide / 14 h / 0 - 20 °C

2.1: NaH / dimethylformamide; various solvent(s) / 0.75 h / 0 - 20 °C

2.2: 45 percent / dimethylformamide; various solvent(s) / 14 h / 20 °C

3.1: HF*pyridine / CH₂Cl₂ / 0 - 20 °C

4.1: 95 percent / pyridine / CH₂Cl₂ / 16 h / 20 °C

With pyridine; sodium hydride; pyridine hydrogenfluoride; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/1099-0690(200208)2002:16<2742::AID-EJOC2742>3.0.CO;2-R