Technology Process of C38H49BrF2N3O9PS
There total 9 articles about C38H49BrF2N3O9PS which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
Rh/Al2O3; hydrogen;
In
ethyl acetate;
for 4h;
under 760.051 Torr;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: 4-methyl-morpholine / tetrahydrofuran / 0.17 h / 0 °C
1.2: 1 h
1.3: 2 h / 20 °C
2.1: Grubbs catalyst first generation / dichloromethane / 17 h / 40 °C / Inert atmosphere; Reflux
2.2: 16 h / Reflux
3.1: Rh/Al2O3; hydrogen / ethyl acetate / 4 h / 760.05 Torr
With
4-methyl-morpholine; Grubbs catalyst first generation; Rh/Al2O3; hydrogen;
In
tetrahydrofuran; dichloromethane; ethyl acetate;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: dichloromethane; 1,4-dioxane / 2 h / 20 °C
1.2: 0.08 h
1.3: 1 h
2.1: lithium hydroxide / water; tetrahydrofuran; methanol / 1 h / 20 °C
3.1: 4-methyl-morpholine / tetrahydrofuran / 0.17 h / 0 °C
3.2: 1 h
3.3: 2 h / 20 °C
4.1: Grubbs catalyst first generation / dichloromethane / 17 h / 40 °C / Inert atmosphere; Reflux
4.2: 16 h / Reflux
5.1: Rh/Al2O3; hydrogen / ethyl acetate / 4 h / 760.05 Torr
With
4-methyl-morpholine; Grubbs catalyst first generation; Rh/Al2O3; hydrogen; lithium hydroxide;
In
tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; water; ethyl acetate;