(2S,3R)-3-(tert-butyldimethylsilyloxy)-6-hydroxy-2-[(R)-1-phenylethylamino]hexyl acetate

Base Information

Chemical Name:(2S,3R)-3-(tert-butyldimethylsilyloxy)-6-hydroxy-2-[(R)-1-phenylethylamino]hexyl acetate
CAS No.:1234672-52-6
Molecular Formula:C₂₂H₃₉NO₄Si
Molecular Weight:409.641
Hs Code.:

Synonyms:(2S,3R)-3-(tert-butyldimethylsilyloxy)-6-hydroxy-2-[(R)-1-phenylethylamino]hexyl acetate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S,3R)-3-(tert-butyldimethylsilyloxy)-6-hydroxy-2-[(R)-1-phenylethylamino]hexyl acetate

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Technology Process of (2S,3R)-3-(tert-butyldimethylsilyloxy)-6-hydroxy-2-[(R)-1-phenylethylamino]hexyl acetate

There total 1 articles about (2S,3R)-3-(tert-butyldimethylsilyloxy)-6-hydroxy-2-[(R)-1-phenylethylamino]hexyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1234672-55-9
(2S,3R)-3,6-bis(tert-butyldimethylsilyloxy)-2-[(R)-1-phenylethylamino]hexyl acetate

: 1234672-52-6
(2S,3R)-3-(tert-butyldimethylsilyloxy)-6-hydroxy-2-[(R)-1-phenylethylamino]hexyl acetate

Guidance literature:: With water; acetic acid; In tetrahydrofuran; at 20 ℃; for 48h; Inert atmosphere;
DOI:10.1016/j.tetlet.2010.04.069

Reference yield: 61.0%

: 1234672-52-6
(2S,3R)-3-(tert-butyldimethylsilyloxy)-6-hydroxy-2-[(R)-1-phenylethylamino]hexyl acetate

: 1234672-56-0
(2S,3R)-3-(tert-butyldimethylsilyloxy)-1-[(R)-1-phenylethylpiperidin-2-yl]methyl acetate

Guidance literature:: With methanesulfonyl chloride; triethylamine; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1016/j.tetlet.2010.04.069