2,3-dihydro-3-methyl-6-(dimethyl(p-nitrophenoxy)methyl)-thiopyran-4-one

Base Information

Chemical Name:2,3-dihydro-3-methyl-6-(dimethyl(p-nitrophenoxy)methyl)-thiopyran-4-one
CAS No.:1033041-99-4
Molecular Formula:C₁₅H₁₇NO₄S
Molecular Weight:307.37
Hs Code.:

Synonyms:2,3-dihydro-3-methyl-6-(dimethyl(p-nitrophenoxy)methyl)-thiopyran-4-one

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Chemical Property of 2,3-dihydro-3-methyl-6-(dimethyl(p-nitrophenoxy)methyl)-thiopyran-4-one

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Technology Process of 2,3-dihydro-3-methyl-6-(dimethyl(p-nitrophenoxy)methyl)-thiopyran-4-one

There total 4 articles about 2,3-dihydro-3-methyl-6-(dimethyl(p-nitrophenoxy)methyl)-thiopyran-4-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: C₁₅H₁₇NO₄S

: 1033041-99-4
2,3-dihydro-3-methyl-6-(dimethyl(p-nitrophenoxy)methyl)-thiopyran-4-one

Guidance literature:: With triethylamine; In N,N-dimethyl-formamide; at 80 ℃; for 6h; Inert atmosphere;
DOI:10.1021/ol800754w

Reference yield: 60.0%

: 115-19-5
2-methyl-but-3-yn-2-ol

: 893445-27-7
S-p-nitrophenyl 2-methylpropanethioate

: 1033041-99-4
2,3-dihydro-3-methyl-6-(dimethyl(p-nitrophenoxy)methyl)-thiopyran-4-one

Guidance literature:: With copper(l) iodide; potassium carbonate; triethylamine; palladium dichloride; In N,N-dimethyl-formamide; at 80 ℃; for 6h; Inert atmosphere;
DOI:10.1021/ol800754w

Reference yield: 51.0%

: 1033042-09-9
C₉H₁₂O₂

: 1849-36-1
para-nitrobenzenethiol

: 1033041-99-4
2,3-dihydro-3-methyl-6-(dimethyl(p-nitrophenoxy)methyl)-thiopyran-4-one

Guidance literature:: With potassium carbonate; triethylamine; In N,N-dimethyl-formamide; at 80 ℃; for 6h; Inert atmosphere;
DOI:10.1021/ol800754w