4-nitrophenyl β-D-fucopyranosyl-(1→4)-β-D-cellobioside

Base Information

Chemical Name:4-nitrophenyl β-D-fucopyranosyl-(1→4)-β-D-cellobioside
CAS No.:1373921-68-6
Molecular Formula:C₂₄H₃₅NO₁₇
Molecular Weight:609.538
Hs Code.:

Synonyms:4-nitrophenyl β-D-fucopyranosyl-(1→4)-β-D-cellobioside

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Chemical Property of 4-nitrophenyl β-D-fucopyranosyl-(1→4)-β-D-cellobioside

Chemical Property:

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Technology Process of 4-nitrophenyl β-D-fucopyranosyl-(1→4)-β-D-cellobioside

There total 14 articles about 4-nitrophenyl β-D-fucopyranosyl-(1→4)-β-D-cellobioside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 3482-57-3
p-nitrophenyl β-D-cellobioside

: 1007855-15-3
α-D-fucopyranosyl fluoride

: 1373921-68-6
4-nitrophenyl β-D-fucopyranosyl-(1→4)-β-D-cellobioside

Guidance literature:: With Thermus nonproteolyticus HG₁₀₂ E₃₃₈A mutant; glycine; sodium hydroxide; In aq. buffer; at 45 ℃; for 48h; pH=8.8; Enzymatic reaction;
DOI:10.1002/ejoc.201201507

Reference yield:

: 2106-10-7
1-deoxy-1-fluoro-α-D-glucose

: 1373921-68-6
4-nitrophenyl β-D-fucopyranosyl-(1→4)-β-D-cellobioside

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydroxide; Thermus nonproteolyticus HG₁₀₂ E₃₃₈A mutant; glycine / aq. buffer / 48 h / 45 °C / pH 8.8 / Enzymatic reaction

2: sodium hydroxide; Thermus nonproteolyticus HG₁₀₂ E₃₃₈A mutant; glycine / aq. buffer / 48 h / 45 °C / pH 8.8 / Enzymatic reaction

With Thermus nonproteolyticus HG₁₀₂ E₃₃₈A mutant; glycine; sodium hydroxide; In aq. buffer;
DOI:10.1002/ejoc.201201507

Reference yield:

: 5328-50-7,5346-90-7,6291-42-5,6920-00-9,20764-63-0,20880-60-8,20880-65-3,22352-19-8,23973-20-8,32447-69-1,34213-32-6,52554-32-2,53956-64-2,56907-29-0,56994-12-8,56994-13-9,57128-38-8,67650-36-6,68036-17-9,68036-19-1,78215-50-6,78215-51-7,79549-48-7,80446-82-8,85249-04-3,93221-83-1,93779-27-2,111407-83-1,111407-84-2,111407-85-3,120328-65-6,123809-59-6,132341-46-9,132341-47-0,132341-49-2,145307-94-4,3616-19-1
D-cellobiose octaacetate

: 1373921-68-6
4-nitrophenyl β-D-fucopyranosyl-(1→4)-β-D-cellobioside

Guidance literature:: Multi-step reaction with 4 steps

1: hydrogen bromide; acetic acid / dichloromethane / 0 - 20 °C

2: tetra(n-butyl)ammonium hydrogensulfate; sodium hydroxide / water; dichloromethane / 20 °C

3: methanol; sodium methylate / 20 °C / pH 10 - 11

4: sodium hydroxide; Thermus nonproteolyticus HG₁₀₂ E₃₃₈A mutant; glycine / aq. buffer / 48 h / 45 °C / pH 8.8 / Enzymatic reaction

With methanol; Thermus nonproteolyticus HG₁₀₂ E₃₃₈A mutant; hydrogen bromide; sodium methylate; tetra(n-butyl)ammonium hydrogensulfate; acetic acid; glycine; sodium hydroxide; In dichloromethane; water;
DOI:10.1002/ejoc.201201507