C₃₀H₂₉BrN₂O₄S

Base Information

Chemical Name:C₃₀H₂₉BrN₂O₄S
CAS No.:957214-75-4
Molecular Formula:C₃₀H₂₉BrN₂O₄S
Molecular Weight:593.541
Hs Code.:

C<sub>30</sub>H<sub>29</sub>BrN<sub>2</sub>O<sub>4</sub>S

Synonyms:C₃₀H₂₉BrN₂O₄S

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Chemical Property of C₃₀H₂₉BrN₂O₄S

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Technology Process of C₃₀H₂₉BrN₂O₄S

There total 2 articles about C₃₀H₂₉BrN₂O₄S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 501-53-1,94274-21-2
benzyl chloroformate

: 107-11-9,30551-89-4
1-amino-2-propene

: 181271-32-9
4-bromo-1-(4-toluenesulfonyl)indole-3-carboxaldehyde

: 1730-25-2
allylmagnesium bromide

: 957214-75-4
C₃₀H₂₉BrN₂O₄S

Guidance literature:: 1-amino-2-propene; 4-bromo-1-(4-toluenesulfonyl)indole-3-carboxaldehyde; With 4 A molecular sieve; In dichloromethane;

allylmagnesium bromide; In tetrahydrofuran;

benzyl chloroformate; Further stages.;
DOI:10.1021/ol7018357

Reference yield:

: C₁₉H₁₇BrN₂O₂S

: 501-53-1,94274-21-2
benzyl chloroformate

: 1730-25-2
allylmagnesium bromide

: 957214-75-4
C₃₀H₂₉BrN₂O₄S

Guidance literature:: C₁₉H₁₇BrN₂O₂S; allylmagnesium bromide; In tetrahydrofuran; diethyl ether; at -78 - 20 ℃; for 1h; Inert atmosphere;

benzyl chloroformate; In tetrahydrofuran; diethyl ether; at -78 - 20 ℃; for 1h; Inert atmosphere;
DOI:10.1016/j.tet.2009.05.009

Reference yield:

: 957214-75-4
C₃₀H₂₉BrN₂O₄S

: C₂₈H₂₄N₂O₄S

Guidance literature:: Multi-step reaction with 2 steps

1: Grubbs catalyst / CH₂Cl₂

2: NEt₃; Bu₄NCl; P(o-tol)3 / Pd(OAc)2 / acetonitrile / 120 °C / microwave irradiation

With tetrabutyl-ammonium chloride; triethylamine; tris-(o-tolyl)phosphine; palladium diacetate; Grubbs catalyst first generation; In dichloromethane; acetonitrile; 2: Heck reaction;
DOI:10.1021/ol7018357