(S)-3-benzyloxy-4-(benzyloxycarbonyl-carbamoylmethyl-amino)butyric acid

Base Information

Chemical Name:(S)-3-benzyloxy-4-(benzyloxycarbonyl-carbamoylmethyl-amino)butyric acid
CAS No.:1431373-86-2
Molecular Formula:C₂₁H₂₄N₂O₆
Molecular Weight:400.431
Hs Code.:

Synonyms:(S)-3-benzyloxy-4-(benzyloxycarbonyl-carbamoylmethyl-amino)butyric acid

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Chemical Property of (S)-3-benzyloxy-4-(benzyloxycarbonyl-carbamoylmethyl-amino)butyric acid

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Technology Process of (S)-3-benzyloxy-4-(benzyloxycarbonyl-carbamoylmethyl-amino)butyric acid

There total 8 articles about (S)-3-benzyloxy-4-(benzyloxycarbonyl-carbamoylmethyl-amino)butyric acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₁H₂₄N₂O₅

: 1431373-86-2
(S)-3-benzyloxy-4-(benzyloxycarbonyl-carbamoylmethyl-amino)butyric acid

Guidance literature:: With sodium chlorite; sodium dihydrogenphosphate dihydrate; In water; tert-butyl alcohol; at 0 - 20 ℃; for 4h; Inert atmosphere;
DOI:10.1016/j.tetlet.2013.03.035

Reference yield:

: C₂₂H₂₈N₂O₆

: 1431373-86-2
(S)-3-benzyloxy-4-(benzyloxycarbonyl-carbamoylmethyl-amino)butyric acid

Guidance literature:: Multi-step reaction with 2 steps

1: sodium periodate / water; methanol / 2 h / 20 °C / Inert atmosphere

2: sodium chlorite; sodium dihydrogenphosphate dihydrate / water; tert-butyl alcohol / 4 h / 0 - 20 °C / Inert atmosphere

With sodium chlorite; sodium periodate; sodium dihydrogenphosphate dihydrate; In methanol; water; tert-butyl alcohol;
DOI:10.1016/j.tetlet.2013.03.035

Reference yield:

: 87604-53-3
(R)-4-((S)-1-(benzyloxy)but-3-ene-1-yl)-2,2-dimethyl-1,3-dioxypentane

: 1431373-86-2
(S)-3-benzyloxy-4-(benzyloxycarbonyl-carbamoylmethyl-amino)butyric acid

Guidance literature:: Multi-step reaction with 8 steps

1: acetic acid / 24 h / 20 °C / Inert atmosphere

2: sodium periodate / water; methanol / 2 h / 20 °C / Inert atmosphere

3: triethylamine / methanol; diethyl ether / 0.17 h / 0 °C / Inert atmosphere

4: sodium cyanoborohydride / methanol; diethyl ether / 4 h / 0 - 20 °C / Inert atmosphere

5: sodium hydrogencarbonate / ethanol; water / 3 h / 0 - 20 °C / Inert atmosphere

6: osmium(VIII) oxide; 4-methylmorpholine N-oxide; water / acetone / 14 h / 20 °C / Inert atmosphere

7: sodium periodate / water; methanol / 2 h / 20 °C / Inert atmosphere

8: sodium chlorite; sodium dihydrogenphosphate dihydrate / water; tert-butyl alcohol / 4 h / 0 - 20 °C / Inert atmosphere

With sodium chlorite; sodium periodate; osmium(VIII) oxide; sodium dihydrogenphosphate dihydrate; water; sodium cyanoborohydride; sodium hydrogencarbonate; acetic acid; 4-methylmorpholine N-oxide; triethylamine; In methanol; diethyl ether; ethanol; water; acetone; tert-butyl alcohol;
DOI:10.1016/j.tetlet.2013.03.035