N-formyl-1,2,3,4,5,6,7,8-octahydro-1-(3'hydroxyphenetyl)-6-oxoisoquinoline

Base Information

• Chemical Name: N-formyl-1,2,3,4,5,6,7,8-octahydro-1-(3'hydroxyphenetyl)-6-oxoisoquinoline
• CAS No.: 106488-64-6
• Molecular Formula: C₁₈H₂₁NO₃
• Molecular Weight: 299.37

Synonyms:N-formyl-1,2,3,4,5,6,7,8-octahydro-1-(3'hydroxyphenetyl)-6-oxoisoquinoline

Chemical Property of N-formyl-1,2,3,4,5,6,7,8-octahydro-1-(3'hydroxyphenetyl)-6-oxoisoquinoline

Chemical Property:

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Technology Process of N-formyl-1,2,3,4,5,6,7,8-octahydro-1-(3'hydroxyphenetyl)-6-oxoisoquinoline

There total 2 articles about N-formyl-1,2,3,4,5,6,7,8-octahydro-1-(3'hydroxyphenetyl)-6-oxoisoquinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

N-formyl-1,2,3,4,5,8-hexahydro-1-(3'hydroxyphenetyl)-6-methoxyisoquinoline → N-formyl-1,2,3,4,5,6,7,8-octahydro-1-(3'hydroxyphenetyl)-6-oxoisoquinoline (106488-64-6)

Guidance literature:

With formic acid; water; In tetrahydrofuran; for 1h; Ambient temperature;

DOI:10.1002/hlca.19850680806

Reference yield:

1,2,3,4,5,8-hexahydro-1-(3'hydroxyphenetyl)-6-methoxyisoquinoline (106488-62-4) → N-formyl-1,2,3,4,5,6,7,8-octahydro-1-(3'hydroxyphenetyl)-6-oxoisoquinoline (106488-64-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 77 percent / 72 h / Heating

2: 84 percent / 88percent HCOOH, H₂O / tetrahydrofuran / 1 h / Ambient temperature

With formic acid; water; In tetrahydrofuran;

DOI:10.1002/hlca.19850680806

Reference yield: 75.0%

N-formyl-1,2,3,4,5,6,7,8-octahydro-1-(3'hydroxyphenetyl)-6-oxoisoquinoline (106488-64-6) → N-formyl-1,2,3,4,6,7,8,8a-octahydro-1-(3'hydroxyphenetyl)-6-oxoisoquinoline (106564-70-9)

Guidance literature:

With trifluorormethanesulfonic acid; for 120h; Ambient temperature;

DOI:10.1002/hlca.19850680806

upstream raw materials:

1,2,3,4,5,8-hexahydro-1-(3'hydroxyphenetyl)-6-methoxyisoquinoline

Downstream raw materials:

N-formyl-1,2,3,4,6,7,8,8a-octahydro-1-(3'hydroxyphenetyl)-6-oxoisoquinoline

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